Integration of high pressure extraction to separation operations for the recovery of by-products from fruit processing

• Grant number: 15/11932-7
• Support Opportunities: Regular Research Grants
• Start date: March 01, 2016
• End date: April 30, 2018
• Field of knowledge: Agronomical Sciences - Food Science and Technology - Food Engineering
• Principal Investigator: Julian Martínez
• Grantee: Julian Martínez
• Host Institution: Faculdade de Engenharia de Alimentos (FEA). Universidade Estadual de Campinas (UNICAMP). Campinas , SP, Brazil
• Associated researchers: Ana Carolina de Aguiar ; Camila Alves de Rezende ; Marcus Bruno Soares Forte ; Marili Villa Nova Rodrigues ; Maurício Ariel Rostagno ; Vera Lúcia Garcia

Abstract

The Laboratory of High Pressure in Food Engineering (LAPEA) has focused its activities on the investigation of high pressure processes, with emphasis in supercritical technology for obtaining high value products from natural sources. Recent results have shown that by-products from the food industry are important sourced of bioactive compounds, and high pressure technologies are viable alternatives for the recovery and purification of those compounds through clean methods, which are also non-aggressive to the environment and the product itself. Nevertheless, the technical and economical viability of such processes depend of their intensification and integration with other operations usually present in an industrial processing line. In particular, one must envisage the development of separation steps that reduce the costs with product purification and solvent recovery. In this context the present proposal suggests the development of equipments to integrate, in a sequential way, high pressure processes (supercritical extraction and pressurized liquid extraction) to well-known separation operations (fractionation at high pressure, membrane filtration and adsorption). The performance of these processes in sequence depends of the adequacy of the proposed separation techniques to high pressure conditions, at which the components of the process equipment need to be more resistant. Each separation process will be applied to a specific by-product from fruit processing (high pressure fractionation for passion fruit bagasse, membrane filtration for grape marc and adsorption for orange residues). The integration of the processes will be evaluated in terms of yield, and physical, chemical and biological properties of the products, and their resulting applicability as ingredients in the formulation of food and other products. (AU)

Scientific publications

(25)

(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)

VIGANO, JULIANE; BRUMER, ISABELA ZABOTI; DE CAMPOS BRAGA, PATRICIA APARECIDA; DA SILVA, JULIANA KELLY; MAROSTICA JUNIOR, MARIO ROBERTO; REYES REYES, FELIX GUILLERMO; MARTINEZ, JULIAN. Pressurized liquids extraction as an alternative process to readily obtain bioactive compounds from passion fruit rinds. FOOD AND BIOPRODUCTS PROCESSING, v. 100, n. A, p. 382-390, OCT 2016. (14/00372-8, 15/11932-7, 13/02203-6)

PASQUEL REATEGUI, JOSE LUIS; FERNANDES, FLAVIA P.; DOS SANTOS, PHILIPE; REZENDE, CAMILA A.; SARTORATTO, ADILSON; QUEIROGA, CARMEN LUCIA; MARTINEZ, JULIAN. Production of copaiba (Copaifera officinalis) oleoresin particles by supercritical fluid extraction of emulsions. JOURNAL OF SUPERCRITICAL FLUIDS, v. 140, p. 364-371, OCT 2018. (16/13602-7, 09/54137-1, 12/22119-7, 15/11932-7)

VITOR PEREIRA, DEBORA TAMIRES; TARONE, ADRIANA GADIOLI; BETIM CAZARIN, CINTHIA BAU; FERNANDEZ BARBERO, GERARDO; MARTINEZ, JULIAN. Pressurized liquid extraction of bioactive compounds from grape marc. Journal of Food Engineering, v. 240, p. 105-113, JAN 2019. (15/11932-7)

PEREIRA, RUBNER GONCALVES; NAKAMURA, RENATO NAOHIRO; NOVA RODRIGUES, MARILI VILLA; FELIPE OSORIO-TOBON, J.; GARCIA, VERA LUCIA; MARTINEZ, JULIAN. Supercritical fluid extraction of phyllanthin and niranthin from Phyllanthus amarus Schum. & Thonn. JOURNAL OF SUPERCRITICAL FLUIDS, v. 127, p. 23-32, SEP 2017. (15/11932-7)

DOS SANTOS, PHILIPE; MEIRELES, M. ANGELA A.; MARTINEZ, JULIAN. Production of isoamyl acetate by enzymatic reactions in batch and packed bed reactors with supercritical CO2. JOURNAL OF SUPERCRITICAL FLUIDS, v. 127, p. 71-80, SEP 2017. (09/54137-1, 15/11932-7)

BAIAO DIAS, ARTHUR LUIZ; DOS SANTOS, PHILIPE; MARTINEZ, JULIAN. Supercritical CO2 technology applied to the production of flavor ester compounds through lipase-catalyzed reaction: A review. JOURNAL OF CO2 UTILIZATION, v. 23, p. 159-178, JAN 2018. (15/11932-7)

LACHOS-PEREZ, D.; TOMPSETT, G. A.; GUERRA, P.; TIMKO, M. T.; ROSTAGNO, M. A.; MARTINEZ, JULIAN; FORSTER-CARNEIRO, T.. Sugars and char formation on subcritical water hydrolysis of sugarcane straw. Bioresource Technology, v. 243, p. 1069-1077, NOV 2017. (15/11932-7, 13/04304-4, 11/19817-1)

PASQUEL REATEGUI, JOSE LUIS; BARRALES, FRANCISCO MANUEL; REZENDE, CAMILA A.; QUEIROGA, CARMEN L.; MARTINEZ, JULIAN. Production of Copaiba oleoresin particles from emulsions stabilized with modified starches. INDUSTRIAL CROPS AND PRODUCTS, v. 108, p. 128-139, DEC 1 2017. (16/13602-7, 15/11932-7)

DA FONSECA MACHADO, ANA PAULA; RUEDA, MIRIAM; FERNANDEZ BARBERO, GERARDO; MARTIN, ANGEL; JOSE COCERO, MARIA; MARTINEZ, JULIAN. Co-precipitation of anthocyanins of the extract obtained from blackberry residues by pressurized antisolvent process. JOURNAL OF SUPERCRITICAL FLUIDS, v. 137, p. 81-92, JUL 2018. (15/11932-7)

BAIAO DIAS, ARTHUR LUIZ; DA CUNHA, GABRIELA NANUNCIO; DOS SANTOS, PHILIPE; MEIRELES, M. ANGELA A.; MARTINEZ, JULIAN. Fusel oil: Water adsorption and enzymatic synthesis of acetate esters in supercritical CO2. JOURNAL OF SUPERCRITICAL FLUIDS, v. 142, p. 22-31, DEC 2018. (15/11932-7)

SUMERE, BEATRIZ ROCCHETTI; DE SOUZA, MARIANA CORREA; DOS SANTOS, MARIANA PACIFICO; NEVES BEZERRA, ROSANGELA MARIA; DA CUNHA, DIOGO THIMOTEO; MARTINEZ, JULIAN; ROSTAGNO, MAURICIO ARIEL. Combining pressurized liquids with ultrasound to improve the extraction of phenolic compounds from pomegranate peel (Punica granatum L.). ULTRASONICS SONOCHEMISTRY, v. 48, p. 151-162, NOV 2018. (16/19930-6, 15/11932-7, 16/06457-0, 16/20016-7)

VIGANO, JULIANE; BRUMER, ISABELA ZABOTI; DE CAMPOS BRAGA, PATRICIA APARECIDA; DA SILVA, JULIANA KELLY; MAROSTICA JUNIOR, MARIO ROBERTO; REYES REYES, FELIX GUILLERMO; MARTINEZ, JULIAN. Pressurized liquids extraction as an alternative process to readily obtain bioactive compounds from passion fruit rinds. FOOD AND BIOPRODUCTS PROCESSING, v. 100, p. 9-pg., 2016-10-01. (14/00372-8, 13/02203-6, 15/11932-7)

DOS SANTOS, PHILIPE; ZABOT, GIOVANI L.; MEIRELES, M. ANGELA A.; MAZUTTI, MARCIO A.; MARTINEZ, JULIAN. Synthesis of eugenyl acetate by,enzymatic reactions in supercritical carbon dioxide. Biochemical Engineering Journal, v. 114, p. 1-9, OCT 15 2016. (09/54137-1, 15/11932-7, 13/02203-6)

DA FONSECA MACHADO, ANA PAULA; DUARTE PEREIRA, ANA LUIZA; FERNANDEZ BARBERO, GERARDO; MARTINEZ, JULIAN. Recovery of anthocyanins from residues of Rubus fruticosus, Vaccinium myrtillus and Eugenia brasiliensis by ultrasound assisted extraction, pressurized liquid extraction and their combination. Food Chemistry, v. 231, p. 1-10, SEP 15 2017. (15/11932-7, 13/02203-6)

DUARTE, SUSAN HARTWIG; DOS SANTOS, PHILIPE; MICHELON, MARIANO; DE PINHO OLIVEIRA, SUMAIMANA MAYA; MARTINEZ, JULIAN; MAUGERI, FRANCISCO. Recovery of yeast lipids using different cell disruption techniques and supercritical CO2 extraction. Biochemical Engineering Journal, v. 125, p. 230-237, SEP 15 2017. (15/11932-7)

GARCIA-MENDOZA, MARIA DEL PILAR; ESPINOSA-PARDO, FABER ARIEL; BASEGGIO, ANDRESSA MARA; FERNANDEZ BARBERO, GERARDO; MAROSTICA JUNIOR, MARIO ROBERTO; ROSTAGNO, MAURICIO ARIEL; MARTINEZ, JULIAN. Extraction of phenolic compounds and anthocyanins from jucara (Euterpe edulis Mart.) residues using pressurized liquids and supercritical fluids. JOURNAL OF SUPERCRITICAL FLUIDS, v. 119, p. 9-16, JAN 2017. (15/11932-7, 13/04304-4, 13/02203-6)

DOS SANTOS, PHILIPE; VIGANO, JULIANE; FURTADO, GUILHERME DE FIGUEIREDO; CUNHA, ROSIANE LOPES; HUBINGER, MIRIAM DUPAS; REZENDE, CAMILA ALVES; MARTINEZ, JULIAN. Production of resveratrol loaded alginate aerogel: Characterization, mathematical modeling, and study of impregnation. JOURNAL OF SUPERCRITICAL FLUIDS, v. 163, SEP 1 2020. (16/02007-0, 15/11932-7, 17/23670-2)

VIGANO, JULIANE; MEIRELLES, AURELIANO A. D.; NATHIA-NEVES, GRAZIELLE; BASEGGIO, ANDRESSA M.; CUNHA, ROSIANE L.; MAROSTICA JUNIOR, MARIO R.; MEIRELES, M. ANGELA A.; GURIKOV, PAVEL; SMIRNOVA, IRINA; MARTINEZ, JULIAN. Impregnation of passion fruit bagasse extract in alginate aerogel microparticles. International Journal of Biological Macromolecules, v. 155, p. 1060-1068, JUL 15 2020. (16/02007-0, 17/18883-7, 17/23670-2, 15/11932-7)

DA FONSECA MACHADO, ANA PAULA; REZENDE, CAMILA ALVES; RODRIGUES, RODNEY ALEXANDRE; FERNANDEZ BARBERO, GERARDO; VIEIRA E ROSA, PAULO DE TARSO; MARTINEZ, JULIAN. Encapsulation of anthocyanin-rich extract from blackberry residues by spray-drying, freeze-drying and supercritical antisolvent. Powder Technology, v. 340, p. 553-562, DEC 2018. (16/13602-7, 15/11932-7, 13/02203-6)

BARRALES, FRANCISCO MANUEL; SILVEIRA, PAULA; MENEZES BARBOSA, PAULA DE PAULA; RUVIARO, AMANDA ROGGIA; PAULINO, BRUNO NICOLAU; PASTORE, GLAUCIA MARIA; MACEDO, GABRIELA ALVES; MARTINEZ, JULIAN. Recovery of phenolic compounds from citrus by-products using pressurized liquids - An application to orange peel. FOOD AND BIOPRODUCTS PROCESSING, v. 112, p. 9-21, NOV 2018. (15/11932-7)

DA FONSECA MACHADO, ANA PAULA; SUMERE, BEATRIZ ROCCHETTI; MEKARU, CAROLINA; MARTINEZ, JULIAN; NEVES BEZERRA, ROSANGELA MARIA; ROSTAGNO, MAURICIO ARIEL. Extraction of polyphenols and antioxidants from pomegranate peel using ultrasound: influence of temperature, frequency and operation mode. INTERNATIONAL JOURNAL OF FOOD SCIENCE AND TECHNOLOGY, v. 54, n. 9, p. 2792-2801, SEP 2019. (15/11932-7, 13/04304-4)

BAIAO DIAS, ARTHUR LUIZ; ARROIO SERGIO, CAMILLA SCARELLI; SANTOS, PHILIPE; BARBERO, GERARDO FERNANDEZ; REZENDE, CAMILA ALVES; MARTINEZ, JULIAN. Ultrasound-assisted extraction of bioactive compounds from dedo de moca pepper (Capsicum baccatum L.): Effects on the vegetable matrix and mathematical modeling. Journal of Food Engineering, v. 198, p. 36-44, APR 2017. (15/11932-7, 13/02203-6)

ESPINOSA-PARDO, FABER ARIEL; NAKAJIMA, VANIA MAYUVNI; MACEDO, GABRIELA ALVES; MACEDO, JULIANA ALVES; MARTINEZ, JULIAN. Extraction of phenolic compounds from dry and fermented orange pomace using supercritical CO2 and cosolvents. FOOD AND BIOPRODUCTS PROCESSING, v. 101, p. 1-10, JAN 2017. (15/11932-7, 13/02203-6)

VIGANO, JULIANE; ZABOT, GIOVANI L.; MARTINEZ, JULIAN. Supercritical fluid and pressurized liquid extractions of phytonutrients from passion fruit by-products: Economic evaluation of sequential multi-stage and single-stage processes. JOURNAL OF SUPERCRITICAL FLUIDS, v. 122, p. 88-98, APR 2017. (14/00372-8, 15/11932-7, 13/02203-6)

LUIS PASQUEL-REATEGUI, JOSE; DOS SANTOS, LUANA CRISTINA; BARRALES, FRANCISCO MANUEL; GROBER, VANESSA LAIS; SOARES FORTE, MARCUS BRUNO; SARTORATTO, ADILSON; QUEIROGA, CARMEN LUCIA; MARTINEZ, JULIAN. Fractionation of sesquiterpenes and diterpenic acids from copaiba (Copaifera officinalis) oleoresin using supercritical adsorption. JOURNAL OF SUPERCRITICAL FLUIDS, v. 184, p. 10-pg., 2022-05-01. (17/23670-2, 15/11932-7, 16/13602-7, 17/11245-5)