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Mult-user equipment approved in the grant 2014/50249-8: ultra-performance liquid chromatography with supercritical CO2 and mass detector

Grant number: 16/20609-8
Support type:Multi-user Equipment Program
Duration: February 01, 2017 - January 31, 2024
Field of knowledge:Physical Sciences and Mathematics - Chemistry
Cooperation agreement: GlaxoSmithKline
Principal Investigator:Arlene Gonçalves Corrêa
Grantee:Arlene Gonçalves Corrêa
Home Institution: Centro de Ciências Exatas e de Tecnologia (CCET). Universidade Federal de São Carlos (UFSCAR). São Carlos , SP, Brazil
Associated research grant:14/50249-8 - Green chemistry: sustainable synthetic methods employing benign solvents, safer reagents, and bio-renewable feedstock, AP.PCPE
As informações de acesso ao Equipamento Multiusuário são de responsabilidade do Pesquisador responsável
EMU web page:http://www.cersuschem.ufscar.br/pesquisa/equipamentos-multiusuario
Tipo de equipamento:Caracterização de Materiais - Análises Químicas - Cromatografia líquida acoplada a espectrômetro de massa
Fabricante: Waters
Modelo: Detector Xevo TQD + Cromatografo Fluído Super Crítico ACQUITY UPC2

Abstract

The purchase of this equipment will be of pivotal importance to all members of the CERSusChem to fulfill their basic needs of research, as the proposal aims the preparation, separation and identification of enantiomerically pure or chiral enriched substances. Therefore, we plan to use the ultra-performance liquid chromatography as analytical tool. This new technology provides both high speed and resolution without sacrificing basic parameters of the analysis. A very important characteristic of this system is the rate at which analysis can be executed - this factor will facilitate the identification and characterization of the synthesized compounds by our staff, and thus, the results can be obtained in a quickly and effectively way. Furthermore, we also have to emphasize that this device has, supercritical CO2 as mobile phase in the presence of small amounts of a co-solvent. This feature avoids the need to purchase special solvents, which are generally expensive, being a waste free apparatus - therefore contributing to the principles of green chemistry. (AU)