Effect of the modification by titanium dioxide nanotubes with different structures on the fatigue response of Ti grade 2

Autor(es)

Leonardo Contri Campanelli ^[1] ; Paulo Sergio Carvalho Pereira da Silva ^[2] ; Nilson Tadeu Camarinho Oliveira ^[3] ; Claudemiro Bolfarini ^[4]

Afiliação do(s) autor(es)

^[1] Federal University of São Carlos. Department of Materials Engineering - Brasil

^[2] Federal University of São Carlos. Department of Materials Engineering - Brasil

^[3] University of São Paulo. Institute of Chemistry of São Carlos - Brasil

^[4] Federal University of São Carlos. Department of Materials Engineering - Brasil

• Tipo de documento: Artigo Científico
• Fonte: MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS; v. 20, p. 120-124, 2017-05-18.

Resumo

Nanotechnology is seeing as having potential to raise benefits to several research and application areas. Recently materials with nanostructured surfaces of nanopores, nanotubes and nanowires have become an important investigation field, since their chemical and physical properties may be substantially different from those of the corresponding substrate. In face of the necessity of assuring that such modifications are not deleterious to the mechanical behavior, the purpose of this work was to evaluate the fatigue performance of CP-Ti grade 2 with the surface modified by the formation of nanotubes on their different crystalline structures. The nanotubes layers were produced by anodic oxidation using a potential of 20V during 1h and a solution of glycerol, H2O and NaF, and analyzed by scanning electron microscopy. In order to obtain the anatase and rutile structures, annealing treatments were respectively performed at 450°C and 650°C. The axial fatigue tests were conducted in physiological solution at 37°C following the stepwise load increase approach. When compared to the material without surface modification (polished surface), the results showed that the anatase phase did not affect the fatigue response, maintaining the fracture stress in 500 MPa, whereas the rutile phase caused a decrease to 450 MPa. (AU)

• Processo FAPESP: 13/04423-3 - Comportamento em fadiga de ligas de titânio beta
• Beneficiário: Leonardo Contri Campanelli
• Linha de fomento: Bolsas no Brasil - Doutorado
• Processo FAPESP: 16/12995-5 - Fadiga de uma liga beta metaestável de titânio para aplicação como biomaterial
• Beneficiário: Leonardo Contri Campanelli
• Linha de fomento: Bolsas no Brasil - Pós-Doutorado
• Processo FAPESP: 12/01652-9 - Desenvolvimento de superfícies nanoestruturadas via eletroquímica em ligas biomédicas de titânio
• Beneficiário: Nilson Tadeu Camarinho de Oliveira
• Linha de fomento: Auxílio à Pesquisa - Apoio a Jovens Pesquisadores