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Mechanical activation of Nb75Al mixtures using shaker and planetary ball mills

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Autor(es):
Rocha, C. J. ; Goncalves, V. S. ; Neto, R. M. Leal ; Salgado, L ; Filho, FA
Número total de Autores: 5
Tipo de documento: Artigo Científico
Fonte: Materials Science Forum; v. 530-531, p. 2-pg., 2006-01-01.
Resumo

Different types of high-energy ball mills can be applied to promote mechanical activation of powders mixtures for further combustion synthesis of intermetallic compounds. In this work, Nb75Al powder mixtures (for NbAl3 synthesis) were mechanically activated in shaker and planetary mills by I and 3 hours. Remarkable differences in shape and microstructure of the activated powders resulted in distinct reaction behaviors (e.g. ignition and combustion temperatures). Temperature profile of the samples during the reaction showed that mechanical activation was higher in the shaker mill. Higher densities were obtained with samples activated in shaker mill by I h. (AU)

Processo FAPESP: 01/03961-4 - Sintese por combustao mecanicamente ativada do trialumineto de niobio , nbal3.
Beneficiário:Ricardo Mendes Leal Neto
Modalidade de apoio: Auxílio à Pesquisa - Regular