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Synthesis of SnSb2Te4 Microplatelets by High-energy Ball Milling

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Autor(es):
da Luz, Mario Sergio ; Tofanello, Fernando Pacheco ; Esposto, Murilo Senhuki ; de Campos, Ariana ; Ferreira, Bento ; Moreira dos Santos, Carlos Alberto
Número total de Autores: 6
Tipo de documento: Artigo Científico
Fonte: MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS; v. 18, n. 5, p. 4-pg., 2015-09-01.
Resumo

In this work we demonstrate that high-energy ball milling process can be used to synthesize SnSb2Te4 without surfactant and further annealing. Milling parameters such as ball to raw material ratio (5:1) and milling time (2h) were determined to be suitable for synthesizing microplatelets of SnSb2Te4. The powders after milling for various durations were characterized by X-ray powder diffraction, scanning electron microscopy and electrical resistance measurements. (AU)

Processo FAPESP: 09/54001-2 - EMU: aquisição de equipamento cryo-free para caracterização de propriedades magnéticas por magnetometria de amostra vibrante (VSM)
Beneficiário:Carlos Alberto Moreira dos Santos
Modalidade de apoio: Auxílio à Pesquisa - Programa Equipamentos Multiusuários