Effects of Sc Addition and Direct Aging Treatment on Microstructure and Hardness of AlSi10Mg Alloy

Autor(es)

Martinez, Fellipe ; dos Santos Junior, Carlos ; Leal, Jaderson ; Silva, Argos ; Gouveia, Guilherme ; Spinelli, Jose

• Tipo de documento: Artigo Científico
• Fonte: ADVANCED ENGINEERING MATERIALS; v. N/A, p. 10-pg., 2023-07-05.

Resumo

Cu-mold centrifugal cast processing is employed as a rapid solidification method for producing samples with and without Sc. The Al-Si-Mg and Al-Si-Mg-Sc alloy samples are exposed to direct aging treatments varying temperature and time to verify the microstructural changes. Both rapidly solidified samples and as-aged samples are characterized by a number of methods, including optical microscopy, SEM-EDS, transmission Electron Microscopy (TEM)-EDS, TEM-HAADF, X-ray diffraction (XRD), differential scanning calorimetry (DSC), and Vickers hardness. At first, the results point to a strong precipitate-related hardening effect formed as a result of the Sc addition to the alloy. All samples containing Sc show a higher hardness value when compared to their respective treated samples without Sc. Second, when comparing the Al-10Si-Mg-0.4Sc alloy samples among themselves after being treated at different conditions, high temperatures, and excessive treatment times are recognized as detrimental to the hardness. This is due to the growth of larger Sc-bearing precipitates of approximately 1 & mu;m in size under such conditions, having lower efficiency in pinning dislocations during loading. The best aging condition is 255 & DEG;C for 60 min, which produces a very fine dispersion of Mg and Sc intermetallics (200 nm in size) with a peak hardness of 110 HV. (AU)

• Processo FAPESP: 19/21937-7 - Efeitos da adição de SC na liga Al-10%Si-Mg para manufatura aditiva e aplicação aeronáutica
• Beneficiário: Fellipe Martinez
• Modalidade de apoio: Bolsas no Brasil - Iniciação Científica
• Processo FAPESP: 21/08436-9 - Eletromigração e microtomografia 4D em juntas térmicas Sn-Bi-In
• Beneficiário: José Eduardo Spinelli
• Modalidade de apoio: Bolsas no Exterior - Pesquisa
• Processo FAPESP: 19/23673-7 - Avaliação de ligas para juntas térmicas e para manufatura aditiva
• Beneficiário: José Eduardo Spinelli
• Modalidade de apoio: Auxílio à Pesquisa - Regular