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(Referência obtida automaticamente do Web of Science, por meio da informação sobre o financiamento pela FAPESP e o número do processo correspondente, incluída na publicação pelos autores.)

X-ray powder diffraction of high-absorption materials at the XRD1 beamline off the best conditions: Application to (Gd, Nd)(5)Si-4 compounds

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Autor(es):
Carvalho, A. M. G. ; Nunes, R. S. ; Coelho, A. A.
Número total de Autores: 3
Tipo de documento: Artigo Científico
Fonte: Powder Diffraction; v. 32, n. 1, p. 10-14, MAR 2017.
Citações Web of Science: 8
Resumo

Representative compounds of the new family of magnetic materials Gd5-xNdxSi4 were analyzed by X-ray diffraction at the XRD1 beamline at Laboratorio Nacional de Luz Sincrotron. To reduce X-ray absorption, thin layers of the powder samples were mounted outside the capillaries and measured in Debye-Scherrer geometry as usual. The XRD analyses and the magnetometry results indicate that the behavior of the magnetic transition temperature as a function of Nd content may be directly related to the average of the four smallest interatomic distances between different rare earth sites of the majority phase of each compound. The quality and consistency of the results show that the XRD1 beamline is able to perform satisfactory XRD experiments on high-absorption materials even off the best conditions. (C) 2016 International Centre for Diffraction Data. (AU)

Processo FAPESP: 12/03480-0 - Efeito magnetocalórico e efeito barocalórico: novas técnicas experimentais, materiais e modelos teóricos
Beneficiário:Alexandre Magnus Gomes Carvalho
Modalidade de apoio: Auxílio à Pesquisa - Jovens Pesquisadores