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(Referência obtida automaticamente do Web of Science, por meio da informação sobre o financiamento pela FAPESP e o número do processo correspondente, incluída na publicação pelos autores.)

Qualitative and Quantitative Chemical Investigation of Orthopedic Alloys by Combining Wet Digestion, Spectroanalytical Methods and Direct Solid Analysis

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Autor(es):
Figueiredo, Caio M. [1] ; Castro, Jeyne P. [1] ; Speranca, Marco A. [1] ; Fialho, Lucimar L. [1] ; Nobrega, Joaquim A. [1] ; Pereira-Filho, Edenir R. [1]
Número total de Autores: 6
Afiliação do(s) autor(es):
[1] Univ Fed Sao Carlos, Dept Quim, GAIA, POB 676, BR-13565905 Sao Carlos, SP - Brazil
Número total de Afiliações: 1
Tipo de documento: Artigo Científico
Fonte: Journal of the Brazilian Chemical Society; v. 29, n. 4, p. 680-688, APR 2018.
Citações Web of Science: 2
Resumo

In this study, two laser-based techniques, laser-induced breakdown spectroscopy (LIBS) and laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) were used for analytical signal evaluation of Ti, Al, and V and investigation of possible harmful elements eventually present as minor elements in Ti alloys. Due to the lack of certified reference materials, samples were also analyzed by wavelength dispersive X-ray fluorescence (WDXRF) and inductively coupled plasma optical emission spectrometry (ICP OES) after microwave-assisted digestion. To maximize the efficiency of LIBS and LA-ICP-MS, operational conditions were adjusted aiming to find optimal analytical performance. LIBS showed several Ti emission lines and few signals for Al and V. LA-ICP-MS was able to detect all three major constituents. For quantitative analysis, the correlation of intensity signals from LIBS analysis with reference values obtained by ICP OES was not successful, showing that there are still difficulties for quantification using solid samples. Measurements using ICP OES showed that additionally to major constituents, only Fe was present in concentrations around 0.2%. Analysis by WDXRF confirmed the presence of Fe. Results using both methods, i.e., ICP OES and WDXRF, were in good agreement. (AU)

Processo FAPESP: 14/22408-4 - Utilização da técnica Laser-Induced Breakdown Spectroscopy (LIBS) para análise direta de amostras de ligas metálicas
Beneficiário:Jeyne Pricylla Castro Castilho
Modalidade de apoio: Bolsas no Brasil - Mestrado
Processo FAPESP: 16/17221-8 - Avaliação da composição de discos rígidos de lixo eletrônico por meio de técnicas espectroanalíticas: determinação de elementos preciosos e terras raras
Beneficiário:Jeyne Pricylla Castro Castilho
Modalidade de apoio: Bolsas no Brasil - Doutorado
Processo FAPESP: 16/01513-0 - Combinação de LIBS (Laser-Induced Breakdown Spectroscopy) e ICP OES (Inductively Coupled Plasma Optical Emission Spectrometry) na análise de amostras de resíduo eletrônico (circuito eletrônico e polímeros), alimentos e líquidas de difícil preparação
Beneficiário:Edenir Rodrigues Pereira Filho
Modalidade de apoio: Auxílio à Pesquisa - Regular