| Texto completo | |
| Autor(es): |
Hyder, Ali
;
Lima, Irlan S.
;
Oliveira, Thawan G.
;
Oliveira, Giovane J.
;
Goncalves, Josue M.
;
Khan, Zahid U.
;
Memon, Ayaz Ali
;
Solangi, Amber Rehana
;
Angnes, Lucio
Número total de Autores: 9
|
| Tipo de documento: | Artigo Científico |
| Fonte: | Talanta; v. 300, p. 9-pg., 2026-04-01. |
| Resumo | |
Monitoring of glucose (Gluc) levels in commercial beverages plays a vital role in preventing and managing diabetic disease effectively in the human body. As a method for monitoring Glu, a bimetallic nickel and cobalt glycerolates decorated with gold (Au@NiCo-Gly) composite was prepared using a solvothermal approach. A series of characterization analytical techniques has been employed to confirm the synthesis of the Au@NiCo-Gly composite, including Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDX). The performance of the electrochemical sensor was evaluated by using CV and EIS in 0.50 M KOH as a supporting electrolyte. The use of these electrodes for FIA-amperometric quantification of glucose was highly efficient for glucose quantification under optimized experimental parameters. The developed sensor demonstrated a low detection limit of 0.0168 mM and a limit of quantification of 0.0560 mM. The practical applicability of the developed sensor was validated by detecting Gluc in beverage samples with recovery rates (111.5 %) falling within acceptable analytical standards. These findings highlight the Au@NiCo-Gly/GCE modified electrode as a promising candidate for efficient, sensitive, and selective monitoring of Gluc in beverage samples. (AU) | |
| Processo FAPESP: | 22/04127-4 - Alfa-hidróxidos metálicos vs. glicerolatos metálicos: síntese, propriedades e aplicações |
| Beneficiário: | Irlan dos Santos Lima |
| Modalidade de apoio: | Bolsas no Brasil - Doutorado Direto |
| Processo FAPESP: | 23/17560-0 - Design de novos compostos de coordenação de alta entropia por spray-drying e seus derivados para conversão e armazenamento de energia |
| Beneficiário: | Josué Martins Gonçalves |
| Modalidade de apoio: | Auxílio à Pesquisa - Jovens Pesquisadores |