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Combinação de LIBS (Laser-Induced Breakdown Spectroscopy) e ICP OES (Inductively Coupled Plasma Optical Emission Spectrometry) na análise de amostras de resíduo eletrônico (circuito eletrônico e polímeros), alimentos e líquidas de difícil preparação

Processo:16/01513-0
Modalidade de apoio:Auxílio à Pesquisa - Regular
Data de Início da vigência: 01 de agosto de 2017
Data de Término da vigência: 31 de julho de 2019
Área do conhecimento:Ciências Exatas e da Terra - Química - Química Analítica
Pesquisador responsável:Edenir Rodrigues Pereira Filho
Beneficiário:Edenir Rodrigues Pereira Filho
Instituição Sede: Centro de Ciências Exatas e de Tecnologia (CCET). Universidade Federal de São Carlos (UFSCAR). São Carlos , SP, Brasil
Município da Instituição Sede:São Carlos
Assunto(s):Espectroscopia de emissão óptica com plasma induzido por laser  Métodos analíticos de preparação de amostras  Resíduos de equipamentos eletroeletrônicos  Alimentos 
Palavra(s)-Chave do Pesquisador:Alimentos | Amostras agroindustriais | Icp Oes | Libs | Lixo eletrônico | Espectroanalítica

Resumo

Este projeto visa a combinação dos resultados obtidos pelas técnicas Inductively Coupled Optical Emission Spectrometry (ICP OES) e Laser-induced breakdown spectroscopy (LIBS) para a análise direta de diversos tipos de amostras, tais como resíduo eletrônico (baterias, polímeros, discos rígidos, telas e circuitos eletrônicos), alimentos (sucos e alimentos fortificados), suplementos minerais e também amostras líquidas de difícil preparação (óleo e mel, por exemplo). Estas amostras apresentam importância ambiental e agroindustrial e os resultados obtidos trarão informações novas sobre a composição das mesmas, bem como a geração de métodos com mínimo ou nenhum preparo de amostra. Além disso, serão utilizadas ferramentas quimiométricas para melhor entendimento dos resultados e tratamento dos dados. (AU)

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Publicações científicas (48)
(Referências obtidas automaticamente do Web of Science e do SciELO, por meio da informação sobre o financiamento pela FAPESP e o número do processo correspondente, incluída na publicação pelos autores)
COSTA, VINICIUS CAMARA; PEREIRA, FABIOLA MANHAS VERBI. Laser-induced breakdown spectroscopy applied to the rapid identification of different types of polyethylene used for toy manufacturing. JOURNAL OF CHEMOMETRICS, v. 34, n. 12, SI, . (19/01102-8, 16/01513-0, 18/18212-8)
COSTA, VINICIUS CAMARA; CARQUEIJA AMORIM, FABIO ALAN; DE BABOS, DIEGO VICTOR; PEREIRA-FILHO, EDENIR RODRIGUES. Direct determination of Ca, K, Mg, Na, P, S, Fe and Zn in bivalve mollusks by wavelength dispersive X-ray fluorescence (WDXRF) and laser-induced breakdown spectroscopy (LIBS). Food Chemistry, v. 273, n. SI, p. 91-98, . (16/01513-0)
ALEXANDRINA, EDUARDO CARLOS; BABOS, DIEGO VICTOR; ANDRADE, DANIEL FERNANDES; COSTA, VINICIUS CAMARA; LUI, ELAINE SCHORNOBAY; CORREA, NIVALDO APARECIDO; AGUIAR, MONICA LOPES; PEREIRA-FILHO, EDENIR RODRIGUES. Particulate matter (PM10) from Sao Carlos-SP (Brazil): spectroanalytical techniques to evaluate and determine chemical elements. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, v. 99, n. 7, . (16/01513-0, 12/14928-2, 16/17304-0)
BABOS, DIEGO VICTOR; COSTA, VINICIUS CAMARA; PEREIRA-FILHO, EDENIR RODRIGUES. Wavelength dispersive X-ray fluorescence (WD-XRF) applied to speciation of sulphur in mineral supplement for cattle: Evaluation of the chemical and matrix effects. Microchemical Journal, v. 147, p. 628-634, . (16/01513-0)
VICTOR BABOS, DIEGO; CRUZ-CONESA, ANDRES; PEREIRA-FILHO, EDENIR RODRIGUES; ANZANO, JESUS M.. Direct determination of Al and Pb in waste printed circuit boards (PCB) by laser-induced breakdown spectroscopy (LIBS): Evaluation of calibration strategies and economic - environmental questions. JOURNAL OF HAZARDOUS MATERIALS, v. 399, . (16/01513-0)
COSTA, VINICIUS CAMARA; BATISTA AQUINO, FRANCISCO WENDEL; PARANHOS, CAIO MARCIO; PEREIRA-FILHO, EDENIR RODRIGUES. Use of laser-induced breakdown spectroscopy for the determination of polycarbonate (PC) and acrylonitrile-butadiene-styrene (ABS) concentrations in PC/ABS plastics from e-waste. WASTE MANAGEMENT, v. 70, p. 212-221, . (13/04688-7, 16/01513-0)
FIGUEIREDO, CAIO M.; CASTRO, JEYNE P.; SPERANCA, MARCO A.; FIALHO, LUCIMAR L.; NOBREGA, JOAQUIM A.; PEREIRA-FILHO, EDENIR R.. Qualitative and Quantitative Chemical Investigation of Orthopedic Alloys by Combining Wet Digestion, Spectroanalytical Methods and Direct Solid Analysis. Journal of the Brazilian Chemical Society, v. 29, n. 4, p. 680-688, . (14/22408-4, 16/17221-8, 16/01513-0)
BABOS, DIEGO VICTOR; COSTA, VINICIUS CAMARA; SPERANCA, MARCO AURELIO; PEREIRA-FILHO, EDENIR RODRIGUES. Direct determination of calcium and phosphorus in mineral supplements for cattle by wavelength dispersive X-ray fluorescence (WD-XRF). Microchemical Journal, v. 137, p. 272-276, . (16/01513-0)
SPERANCA, MARCO AURELIO; ANDRADE, DANIEL FERNANDES; CASTRO, JEYNE PRICYLLA; PEREIRA-FILHO, EDENIR RODRIGUES. Univariate and multivariate calibration strategies in combination with laser-induced breakdown spectroscopy (LIBS) to determine Ti on sunscreen: A different sample preparation procedure. OPTICS AND LASER TECHNOLOGY, v. 109, p. 648-653, . (16/01513-0, 16/17304-0, 16/17221-8)
GAMELA, RAIMUNDO R.; SPERANCA, MARCO A.; ANDRADE, DANIEL F.; PEREIRA FILHO, EDENIR R.. Hyperspectral images: a qualitative approach to evaluate the chemical profile distribution of Ca, K, Mg, Na and P in edible seeds employing laser-induced breakdown spectroscopy. ANALYTICAL METHODS, v. 11, n. 43, p. 5543-5552, . (16/17304-0, 16/01513-0)
COSTA, VINICIUS C.; PINHEIRO, FERNANDA C.; AMORIM, FABIO ALAN C.; PARANHOS DA SILVA, ERIK G.; PEREIRA-FILHO, EDENIR R.. Multivariate optimization for the development of a sample preparation procedure and evaluation of calibration strategies for nutrient elements determination in handmade chocolate. Microchemical Journal, v. 150, . (16/01513-0)
ZANETTI, T. C.; CATELANI, T. A.; PEREIRA-FILHO, E. R.; CABRAL, J. S.. Laser-induced breakdown spectroscopy as a tool for homogeneity measurements in medicine tablets. Laser Physics, v. 30, n. 3, . (16/01513-0)
ANDRADE, DANIEL FERNANDES; MACHADO, RAQUEL CARDOSO; PEREIRA-FILHO, EDENIR RODRIGUES. Proposition of electronic waste as a reference material - part 2: homogeneity, stability, characterization, and uncertainties. Journal of Analytical Atomic Spectrometry, v. 34, n. 12, p. 2402-2410, . (16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; DE ALMEIDA, EDUARDO; PEREIRA DE CARVALHO, HUDSON WALLACE; PEREIRA-FILHO, EDENIR RODRIGUES; AMARASIRIWARDENA, DULASIRI. Chemical inspection and elemental analysis of electronic waste using data fusion - Application of complementary spectroanalytical techniques. Talanta, v. 225, . (16/01513-0, 15/05942-0, 16/17304-0, 18/24569-6, 19/24223-5)
ANDRADE, DANIEL FERNANDES; PEREIRA-FILHO, EDENIR RODRIGUES; AMARASIRIWARDENA, DULASIRI. Current trends in laser-induced breakdown spectroscopy: a tutorial review. APPLIED SPECTROSCOPY REVIEWS, v. 56, n. 2, . (18/24569-6, 16/17304-0, 16/01513-0)
RAIMUNDO R. GAMELA; VINICIUS C. COSTA; MATHEUS L. DE MELLO; JULIA C. ROMERO; FÁBIO A. C. AMORIM; EDENIR R. PEREIRA-FILHO. Multivariate Analysis: Use of Doehlert Design (DD) for Optimization of a Simple Sample Preparation Procedure for the Determination of Inorganic Constituents in Cocoa Beans Employing Microwave Acid Digestion and ICP OES. Journal of the Brazilian Chemical Society, v. 31, n. 10, p. 2082-2090, . (16/01513-0)
VINICIUS C. COSTA; DIEGO V. BABOS; JEYNE P. CASTRO; DANIEL F. ANDRADE; RAIMUNDO R. GAMELA; RAQUEL C. MACHADO; MARCO A. SPERANÇA; ALISSON S. ARAÚJO; JOSÉ A. GARCIA; EDENIR R. PEREIRA-FILHO. Calibration Strategies Applied to Laser-Induced Breakdown Spectroscopy: A Critical Review of Advances and Challenges. Journal of the Brazilian Chemical Society, v. 31, n. 12, p. 2439-2451, . (16/17221-8, 19/24223-5, 18/17753-5, 18/24569-6, 16/01513-0, 16/17304-0)
MACHADO, RAQUEL C.; BABOS, DIEGO VICTOR; ANDRADE, DANIEL F.; PEREIRA-FILHO, EDENIR RODRIGUES. A novel strategy for direct elemental determination using laser-induced breakdown spectroscopy: fluence calibration. Journal of Analytical Atomic Spectrometry, v. 36, n. 10, . (16/17304-0, 19/24223-5, 16/01513-0)
NEIVA, ARIANE MACIEL; PEREIRA-FILHO, EDENIR RODRIGUES. Evaluation of the Chemical Composition of Synthetic Leather Using Spectroscopy Techniques. Applied Spectroscopy, v. 72, n. 6, p. 921-932, . (11/51564-6, 15/14488-0, 16/01513-0)
BABOS, DIEGO VICTOR; CASTRO, JEYNE PRICYLLA; ANDRADE, DANIEL FERNANDES; COSTA, VINICIUS CAMARA; PEREIRA-FILHO, EDENIR RODRIGUES. Determination and speciation of phosphorus in fertilizers and mineral supplements for cattle by X-ray absorption near-edge structure spectroscopy: a simple nondestructive method. ANALYTICAL METHODS, v. 11, n. 11, p. 1508-1515, . (16/17221-8, 16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; FORTUNATO, FELIPE MANFROI; PEREIRA-FILHO, EDENIR RODRIGUES. Calibration strategies for determination of the In content in discarded liquid crystal displays (LCD) from mobile phones using laser-induced breakdown spectroscopy (LIBS). Analytica Chimica Acta, v. 1061, p. 42-49, . (16/01513-0, 16/17304-0)
COSTA, VINICIUS CAMARA; DE BABOS, DIEGO VICTOR; BATISTA DE AQUINO, FRANCISCO WENDEL; VIRGILIO, ALEX; CARQUEIJA AMORIM, FABIO ALAN; PEREIRA-FILHO, EDENIR RODRIGUES. Direct Determination of Ca, K and Mg in Cassava Flour Samples by Laser-Induced Breakdown Spectroscopy (LIBS). FOOD ANALYTICAL METHODS, v. 11, n. 7, SI, p. 1886-1896, . (16/01513-0)
FABÍOLA MANHAS VERBI PEREIRA; EDENIR RODRIGUES PEREIRA-FILHO. APLICAÇÃO DE PROGRAMA COMPUTACIONAL LIVRE EM PLANEJAMENTO DE EXPERIMENTOS: UM TUTORIAL. Química Nova, v. 41, n. 9, p. 1061-1071, . (16/00779-6, 16/01513-0, 17/05550-0)
AUGUSTO, AMANDA S.; CASTRO, JEYNE P.; SPERANCA, MARCO A.; PEREIRA-FILHO, EDENIR R.. Combination of Multi-Energy Calibration (MEC) and Laser-Induced Breakdown Spectroscopy (LIBS) for Dietary Supplements Analysis and Determination of Ca, Mg and K. Journal of the Brazilian Chemical Society, v. 30, n. 4, p. 804-812, . (16/17221-8, 16/01513-0, 14/11415-0)
SPERANCA, MARCO AURELIO; VIRGILIO, ALEX; PEREIRA-FILHO, EDENIR RODRIGUES; BATISTA DE AQUINO, FRANCISCO WENDEL. Determination of Elemental Content in Solder Mask Samples Used in Printed Circuit Boards Using Different Spectroanalytical Techniques. Applied Spectroscopy, v. 72, n. 8, p. 1205-1214, . (14/18393-1, 13/04688-7, 16/01513-0)
CASTRO, JEYNE PRICYLLA; PEREIRA-FILHO, EDENIR RODRIGUES. Spectroanalytical method for evaluating the technological elements composition of magnets from computer hard disks. Talanta, v. 189, p. 205-210, . (14/22408-4, 16/17221-8, 16/01513-0, 12/50827-6, 12/01769-3)
NEIVA, ARIANE MACIEL; SPERANCA, MARCO AURELIO; COSTA, VINICIUS CAMARA; CHAGAS JACINTO, MANUEL ANTONIO; PEREIRA-FILHO, EDENIR RODRIGUES. Determination of toxic metals in leather by wavelength dispersive X-ray fluorescence (WDXRF) and inductively coupled plasma optical emission spectrometry (ICP OES) with emphasis on chromium. ENVIRONMENTAL MONITORING AND ASSESSMENT, v. 190, n. 10, . (16/01513-0, 11/51564-6, 15/14488-0)
COSTA, VINICIUS CAMARA; CASTRO, JEYNE PRICYLLA; ANDRADE, DANIEL FERNANDES; BABOS, DIEGO VICTOR; GARCIA, JOSE AUGUSTO; SPERANCA, MARCO AURELIO; CATELANI, TIAGO AUGUSTO; PEREIRA-FILHO, EDENIR RODRIGUES. Laser-induced breakdown spectroscopy (LIBS) applications in the chemical analysis of waste electrical and electronic equipment (WEEE). TRAC-TRENDS IN ANALYTICAL CHEMISTRY, v. 108, p. 65-73, . (16/17221-8, 16/17304-0, 16/01513-0)
BABOS, DIEGO VICTOR; VIRGILIO, ALEX; COSTA, VINICIUS CAMARA; DONATI, GEORGE LUIS; PEREIRA-FILHO, EDENIR RODRIGUES. Multi-energy calibration (MEC) applied to laser-induced breakdown spectroscopy (LIBS). Journal of Analytical Atomic Spectrometry, v. 33, n. 10, p. 1753-1762, . (14/18393-1, 16/01513-0)
BABOS, DIEGO VICTOR; BARROS, ARIANE ISIS; NOBREGA, JOAQUIM ARAUJO; PEREIRA-FILHO, EDENIR RODRIGUES. Calibration strategies to overcome matrix effects in laser-induced breakdown spectroscopy: Direct calcium and phosphorus determination in solid mineral supplements. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v. 155, p. 90-98, . (16/01513-0)
COSTA, VINICIUS CAMARA; CARQUEIJA AMORIM, FABIO ALAN; DE BABOS, DIEGO VICTOR; PEREIRA-FILHO, EDENIR RODRIGUES. Direct determination of Ca, K, Mg, Na, P, S, Fe and Zn in bivalve mollusks by wavelength dispersive X-ray fluorescence (WDXRF) and laser-induced breakdown spectroscopy (LIBS). Food Chemistry, v. 273, p. 8-pg., . (16/01513-0)
COSTA, VINICIUS CAMARA; DE BABOS, DIEGO VICTOR; BATISTA DE AQUINO, FRANCISCO WENDEL; VIRGILIO, ALEX; CARQUEIJA AMORIM, FABIO ALAN; PEREIRA-FILHO, EDENIR RODRIGUES. Direct Determination of Ca, K and Mg in Cassava Flour Samples by Laser-Induced Breakdown Spectroscopy (LIBS). FOOD ANALYTICAL METHODS, v. 11, n. 7, p. 11-pg., . (16/01513-0)
VINICIUS C. COSTA; AMANDA S. AUGUSTO; JEYNE P. CASTRO; RAQUEL C. MACHADO; DANIEL F. ANDRADE; DIEGO V. BABOS; MARCO A. SPERANÇA; RAIMUNDO R. GAMELA; EDENIR R. PEREIRA-FILHO. LASER INDUCED-BREAKDOWN SPECTROSCOPY (LIBS): HISTÓRICO, FUNDAMENTOS, APLICAÇÕES E POTENCIALIDADES. Química Nova, v. 42, n. 5, p. 527-545, . (16/17304-0, 14/11415-0, 16/17221-8, 16/01513-0)
CASTRO, JEYNE PRICYLLA; SPERANCA, MARCO AURELIO; BABOS, DIEGO VICTOR; ANDRADE, DANIEL FERNANDES; PEREIRA-FILHO, EDENIR RODRIGUES. Neodymium determination in hard drive disks magnets using different calibration approaches for wavelength dispersive X-ray fluorescence. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v. 164, . (16/01513-0, 16/17304-0, 12/50827-6, 16/17221-8, 18/17753-5, 14/22408-4, 12/01769-3)
COSTA, V. C.; FERREIRA, S. DOS SANTOS; SANTOS, L. N.; SPERANCA, M. A.; DA SILVA, C. SANTOS; SODRE, G. A.; PEREIRA-FILHO, E. R.. Qualitative and Quantitative Analysis of Soils Using Laser-Induced Breakdown Spectroscopy and Chemometrics Tools. Journal of Applied Spectroscopy, v. 87, n. 2, p. 378-386, . (16/01513-0)
ANDRADE, DANIEL FERNANDES; MACHADO, RAQUEL CARDOSO; BACCHI, MARCIO ARRUDA; PEREIRA-FILHO, EDENIR RODRIGUES. Proposition of electronic waste as a reference material - part 1: sample preparation, characterization and chemometric evaluation. Journal of Analytical Atomic Spectrometry, v. 34, n. 12, p. 2394-2401, . (16/01513-0, 16/17304-0)
MACHADO, RAQUEL C.; ANDRADE, DANIEL F.; BABOS, V, DIEGO; CASTRO, JEYNE P.; COSTA, VINICIUS C.; SPERANCA, MARCO AURELIO; GARCIA, JOSE AUGUSTO; GAMELA, RAIMUNDO R.; PEREIRA-FILHO, EDENIR R.. Solid sampling: advantages and challenges for chemical element determination-a critical review. Journal of Analytical Atomic Spectrometry, v. 35, n. 1, p. 54-77, . (16/17221-8, 16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; ROMANELLI, JOAO PAULO; PEREIRA-FILHO, EDENIR RODRIGUES. Past and emerging topics related to electronic waste management: top countries, trends, and perspectives. Environmental Science and Pollution Research, v. 26, n. 17, p. 17135-17151, . (16/17304-0, 16/01513-0)
JIMENEZ, VICTORIA C.; MONFERRAN, MATEO D.; SPERANCA, MARCO A.; CASTRO, JEYNE P.; CATELANI, TIAGO A.; PELLERANO, ROBERTO G.; PERINO, ERNESTO; PEREIRA-FILHO, EDENIR R.; CABALERI, NORA G.; GALLEGO, OSCAR F.. Combination of analytic techniques to chemical characterization and preservation of Jurassic clam shrimp carapaces from La Matilde Formation, Patagonia. Journal of South American Earth Sciences, v. 109, . (14/22408-4, 12/01769-3, 16/17221-8, 12/50827-6, 16/01513-0)
GAMELA, RAIMUNDO R.; COSTA, VINICIUS C.; SPERANCA, MARCO A.; PEREIRA-FILHO, EDENIR R.. Laser-induced breakdown spectroscopy (LIBS) and wavelength dispersive X-ray fluorescence (WDXRF) data fusion to predict the concentration of K, Mg and P in bean seed samples. Food Research International, v. 132, . (16/01513-0)
COSTA, VINICIUS CAMARA; PEREIRA, FABIOLA MANHAS VERBI. Laser-induced breakdown spectroscopy applied to the rapid identification of different types of polyethylene used for toy manufacturing. JOURNAL OF CHEMOMETRICS, v. 34, n. 12, p. 8-pg., . (16/01513-0, 19/01102-8, 18/18212-8)
RIBEIRO, MATHEUS C. S.; SENESI, GIORGIO S.; CABRAL, JADER S.; CENA, CICERO; MARANGONI, BRUNO S.; KIEFER, CHARLES; NICOLODELLI, GUSTAVO. Evaluation of rice varieties using LIBS and FTIR techniques associated with PCA and machine learning algorithms. APPLIED OPTICS, v. 59, n. 32, p. 10043-10048, . (16/01513-0)
NICOLODELLI, GUSTAVO; SCHNEIDER, RICARDO; DOS SANTOS, BRENDA M.; PONTES, GUSTAVO; CABRAL, JADER. Influence of excitation wavelength on LIBS (1064 nm vs 266 nm) for multi-element mortar analysis. Microchemical Journal, v. 207, p. 7-pg., . (16/01513-0)
FERREIRA, DENNIS SILVA; PEREIRA-FILHO, EDENIR RODRIGUES. A preliminary study of a sequential leaching process to recover Ag, Au, Cu, and Sn from E-waste. HYDROMETALLURGY, v. 235, p. 10-pg., . (16/01513-0, 19/24223-5)
ARAUJO, ALISSON SILVA; CASTRO, JEYNE PRICYLLA; SPERANCA, MARCO AURELIO; ANDRADE, DANIEL FERNANDES; DE MELLO, MATHEUS LIMA; PEREIRA-FILHO, EDENIR RODRIGUES. Multiway Calibration Strategies in Laser-Induced Breakdown Spectroscopy: A Proposal. Analytical Chemistry, v. 93, n. 16, p. 10-pg., . (16/01513-0, 16/17304-0, 16/17221-8, 19/24223-5)