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Synthesis of heterocyclic compounds for biological and technological applications

Grant number:18/00544-4
Support Opportunities:Regular Research Grants
Start date: July 01, 2018
End date: September 30, 2020
Field of knowledge:Physical Sciences and Mathematics - Chemistry - Organic Chemistry
Principal Investigator:Rosangela da Silva de Laurentiz
Grantee:Rosangela da Silva de Laurentiz
Host Institution: Faculdade de Engenharia (FEIS). Universidade Estadual Paulista (UNESP). Campus de Ilha Solteira. Ilha Solteira , SP, Brazil
City of the host institution:Ilha Solteira

Abstract

The increasing demand for small organic molecules for use in the development of new drugs and new materials has increased interest in the synthesis of compounds containing functionalized heterocyclic nucleus. A large number of heterocyclic derivatives have been synthesized in the last decades through several synthetic routes, in order to obtain compounds that are more active and establish the relationship between the structures and their physical, chemical and biological properties. However, it is still necessary to propose new synthetic routes or adaptations of routes already known, to obtain compounds of differentiated structures, by combining two or more pharmacophoric groups, for the biological applications, and the combination between carbonic structure and chromophores for application in light emitting devices. Therefore, this research project aims to study the production of heterocyclic compounds derived from piperazines, quinoxolines, pyrimidines, chromenes, diazepines, acridones and acridines, containing a lactonic ring and together substituents donors and acceptors of H. For this will be studied synthetic routes via domino and multicomponent reactions, which will be optimized by the use of various solvents, catalytic systems and microwave irradiation, in order to obtain these derivatives more efficiently. Several heterocyclic compounds to be obtained in this proposal have both structural characteristics present in bioactive compounds and in compounds with luminescent properties. All the products obtained will have their structures confirmed by NMR and MS analysis. The compounds will also undergo biological evaluation and UV / Vis / fluorescence studies. Biological assays will be carried out in collaboration with researchers from Universidade Nova de Lisboa and the Universidade de Franca with which our group has several collaboration projects and published works. (AU)

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Scientific publications (7)
(The scientific publications listed on this page originate from the Web of Science or SciELO databases. Their authors have cited FAPESP grant or fellowship project numbers awarded to Principal Investigators or Fellowship Recipients, whether or not they are among the authors. This information is collected automatically and retrieved directly from those bibliometric databases.)
FINENCIO, BEATRIZ MIORIN; SANTOS, FERNANDA AMORIM; PARREIRA, RENATO LUIS TAME; ORENHA, RENATO PEREIRA; LIMA, SANDRO MARCIO; ANDRADE, LUIS HUMBERTO CUNHA; VENTURA, MARYLEIDE; DE LAURENTIZ, ROSANGELA DA SILVA. Luminescent Properties of β-(hydroxyaryl)-butenolides and Fluorescence Quenching in Water. Journal of Fluorescence, v. N/A, p. 16-pg., . (18/00544-4)
SANTOS, FERNANDA AMORIM; TONDATO, WELLINGTON NEGRI; TAME PARREIRA, RENATO LUIS; ORENHA, RENATO PEREIRA; LEITE LOURENCO, LUIZ CARLOS; DE LAURENTIZ, ROSANGELA DA SILVA. Synthesis and luminescent properties of new naphthoquinoline lactone derivatives. Journal of Luminescence, v. 227, p. 8-pg., . (18/00544-4)
SANCHEZ, CLARA DE ARAUJO; GONCALVES, JULIANA ALENCAR; ANDRADE E SILVA, MARCIO LUIS; RODRIGUES, MARIA GABRIELA FONTANETTI; SANTOS, FERNANDA AMORIM; DE LAURENTIZ, ROSANGELA DA SILVA; DE SOUTELLO, RICARDO VELLUDO GOMES. In vivo anthelmintic activity of hydroethanolic extract of Piper cubeba fruits in sheep naturally infected with gastrointestinal nematodes. Veterinary Parasitology, v. 333, p. 6-pg., . (18/00544-4)
GOMES, ANA CAROLINA; BORGES, ALEXANDRE; ZOCA, DANIELA GARCIA; ANDRADE E SILVA, MARCIO LUIS; DA SILVA RODRIGUES MACHADO, ALINE RAFAELA; MACHADO, ALEX MARTINS; SANTOS, MARIO F. C.; DE LAURENTIZ, ROSANGELA DA SILVA. Larvicidal potential of extracts and isolated compounds from Piper cubeba fruits against Aedes aegypti (Diptera: Culicidae) larvae. NATURAL PRODUCT RESEARCH, v. N/A, p. 8-pg., . (18/00544-4)
BORGES, ALEXANDRE; DE OLIVEIRA, IVAN PIRES; LESCANO, CAROLINE HONAISER; PARREIRA, RENATO LUIS TAME; ORENHA, RENATO PEREIRA; DE LAURENTIZ, ROSANGELA DA SILVA. Molecular interaction analysis of the lignans from Piper cubeba in complex with Haemonchus contortus phosphomethyltransferase. Veterinary Parasitology, v. 321, p. 12-pg., . (18/00544-4, 11/07623-8)
DARON, ERIKA C. A. S. K.; NEGRI, WELLINGTON T.; BORGES, ALEXANDRE; LESCANO, CAROLINE H.; ANTUNES, EDSON; DE LAURENTIZ, ROSANGELA S.. Design, synthesis, and in vitro antiplatelet aggregation activities of taiwanin C. NATURAL PRODUCT RESEARCH, v. N/A, p. 7-pg., . (18/00544-4)
FINENCIO, BEATRIZ M.; SANTOS, FERNANDA A.; LAURENTIZ, ROSANGELA S.. Synthesis of beta-Arylbutenolides Mediated by BF3 center dot OMe2. Synlett, v. 34, n. 01, p. 4-pg., . (18/00544-4)