Microhardness and EBSD Microstructure Mapping in Partially-pressed Al and Cu through 90 degrees ECAP Die

Author(s)

Zhilyaev, Alexander P. ; Langdon, Terence G.

• Document type: Journal article
• Source: MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS; v. 16, n. 3, p. 6-pg., 2013-05-01.

Abstract

Equal-channel angular pressing (ECAP) is widely recognized as an effective method for processing ultrafine-grained and even nanostructured materials. Important details on processes occurring in the die intersections can be obtained by mapping the microhardness and EBSD microstructures in partially-pressed aluminum and copper through the 90 degrees die of ECAP. Precise measurements were made using grids of partially-pressed Al and Cu and detailed color maps were plotted and compared with EBSD maps. A narrow region along the bisector of two channels reflects altering in microhardness level of the material subjected to simple shear. The microstructural evolution suggests significant refining of the grain structure but there is noticeable inhomogeneity in the microhardness and microstructure for both materials. Factors contributing to the inhomogeneous hardness distribution include the coarse initial grain size, and inhomogeneous deformation across the plane of the die channel intersection due to die wall friction and the formation of a dead zone at the outer corner. (AU)

• FAPESP's process: 11/51245-8 - Grain refinement and properties of ultrafine-grained AI, Mg and Ti alloys produced by equal-channel angular pressing with back-pressure
• Grantee: Alberto Moreira Jorge Junior
• Support Opportunities: Regular Research Grants