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Synthesis of SnSb2Te4 Microplatelets by High-energy Ball Milling

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Author(s):
da Luz, Mario Sergio ; Tofanello, Fernando Pacheco ; Esposto, Murilo Senhuki ; de Campos, Ariana ; Ferreira, Bento ; Moreira dos Santos, Carlos Alberto
Total Authors: 6
Document type: Journal article
Source: MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS; v. 18, n. 5, p. 4-pg., 2015-09-01.
Abstract

In this work we demonstrate that high-energy ball milling process can be used to synthesize SnSb2Te4 without surfactant and further annealing. Milling parameters such as ball to raw material ratio (5:1) and milling time (2h) were determined to be suitable for synthesizing microplatelets of SnSb2Te4. The powders after milling for various durations were characterized by X-ray powder diffraction, scanning electron microscopy and electrical resistance measurements. (AU)

FAPESP's process: 09/54001-2 - Acquisition of cryogen-free equipment for the characterization of magnetic properties by vibrating sample magnetometry
Grantee:Carlos Alberto Moreira dos Santos
Support Opportunities: Multi-user Equipment Program