Obtaining annatto seed oil miniemulsions by ultrasonication using aqueous extract from Brazilian ginseng roots as a biosurfactant

Autor(es)

Rosa, M. Thereza M. G. ^[1] ; Silva, Eric Keven ^[1] ; Santos, Diego T. ^[1] ; Petenate, Ademir J. ^[2] ; Meireles, M. Angela A. ^[1]

Afiliação do(s) autor(es)

^[1] UNICAMP Univ Campinas, Sch Food Engn, LASEFI DEA FEA, BR-13083862 Campinas, SP - Brazil

^[2] IMEC UNICAMP, DE, BR-13083970 Campinas, SP - Brazil

• Tipo de documento: Artigo Científico
• Fonte: Journal of Food Engineering; v. 168, p. 68-78, JAN 2015.
• Citações Web of Science: 11

Resumo

The purpose of this study was to produce an oil-in-water (O/W) emulsion of delta-tocotrienol-rich oil obtained from annatto seeds by a supercritical fluid extraction process. The effects of emulsification by ultrasound (US) were evaluated and compared to emulsification by dispax reactor (DR) at similar energy densities. Saponin-rich extract from Brazilian ginseng roots (BGR) was obtained from BGR by pressurized liquid extraction and used as a biosurfactant. A model O/W emulsion system was prepared with soybean oil and commercial saponin. The influence of the emulsification process, energy density, oil type, biosurfactant type and biosurfactant concentration on the size and stability of the resulting droplets was examined through the experimental design and proper statistical analysis. The results showed that US produced more stable emulsion with smaller droplet sizes in comparison with the DR device at the same energy density. In general, increasing the energy density helped to reduce the emulsion droplet size. The minimum average droplet size observed in the mini-emulsions was 0.35 mu m. The data show that both biosurfactants were capable of forming emulsions containing relatively small droplets (<0.83 um) and were rather stable (96-99%), with some creaming. The emulsion droplets also showed a surface potential of approximately 49 mV because of the adsorbed biosurfactants, which minimized the flocculation of the oil droplets. These results indicate that BGR-extracted saponin might be an attractive biosurfactant choice for emulsion formulations for use in food and beverage products. (C) 2015 Elsevier Ltd. All rights reserved. (AU)

• Processo FAPESP: 09/17234-9 - Obtenção de antocianinas, carotenóides, flavonóides, óleos voláteis e tocotrienóis por tecnologia supercrítica: parâmetros de processo e caracterização química
• Beneficiário: Maria Angela de Almeida Meireles Petenate
• Modalidade de apoio: Auxílio à Pesquisa - Regular
• Processo FAPESP: 12/10685-8 - Combinação/acoplamento de processos para a produção e encapsulamento de extratos vegetais de alto valor agregado: avaliação técnica e econômica
• Beneficiário: Maria Angela de Almeida Meireles Petenate
• Modalidade de apoio: Auxílio à Pesquisa - Regular
• Processo FAPESP: 12/19304-7 - Biorrefinaria do ginseng brasileiro: simulação e otimização multiobjetivo
• Beneficiário: Diego Tresinari dos Santos
• Modalidade de apoio: Bolsas no Exterior - Estágio de Pesquisa - Pós-Doutorado
• Processo FAPESP: 10/16485-5 - Avaliação técnica e econômica da integração de processos sustentáveis visando um melhor aproveitamento do ginseng brasileiro (Pfaffia glomerata)
• Beneficiário: Diego Tresinari dos Santos
• Modalidade de apoio: Bolsas no Brasil - Pós-Doutorado