| Full text | |
| Author(s): |
Rotta, Maycon
[1, 2]
;
Motta, Maycon
[3]
;
Pessoa, Alexsander Lourenco
[1]
;
Carvalho, Claudio Luiz
[1]
;
Deimling, Cesar Vanderlei
[4]
;
Lisboa-Filho, Paulo Noronha
[5]
;
Ortiz, Wilson Aires
[3]
;
Zadorosny, Rafael
[1]
Total Authors: 8
|
| Affiliation: | [1] Univ Estadual Paulista, Fac Engn, UNESP, Dept Fis & Quim, Caixa Postal 31, BR-15385000 Ilha Solteira, SP - Brazil
[2] Inst Fed Educ Ciencia & Tecnol Mato Grosso do Sul, Campus Tres Lagoas, BR-79641162 Tres Lagoas, MS - Brazil
[3] Univ Fed Sao Carlos UFSCar, Dept Fis, BR-13565905 Sao Carlos, SP - Brazil
[4] Univ Tecnol Fed Parana UTFPR, Dept Acad Fis, BR-87301899 Campo Mourao, PR - Brazil
[5] Univ Estadual Paulista, Fac Ciencias, Dept Fis, UNESP, Caixa Postal 473, BR-17033360 Bauru, SP - Brazil
Total Affiliations: 5
|
| Document type: | Journal article |
| Source: | Materials Chemistry and Physics; v. 243, MAR 1 2020. |
| Web of Science Citations: | 0 |
| Abstract | |
There are a variety of chemical routes used to produce advanced ceramic materials. The sol-gel-like methods are widely applied since the final samples present high stoichiometric and grain size homogeneity. However, with the search for sustainable practices, researchers have been worked in the so-called one-pot synthesis, where all the chemical reactions occur in a single vessel with low residue production. Thus, in this work, we used a onepot-like synthesis adapted to produce YBa2Cu3O7-delta superconducting ceramic samples. One shows that, in two main steps, a polymer solution is prepared in a few hours, and after heat treatments, a single-phase material is obtained. It is shown that the one-pot-like samples can present a higher diamagnetic signal in comparison with specimens prepared by the well-known Pechini Method. With this work, we show that there are alternative routes to produce advanced ceramics with simple and secure methods, if we compare, e.g., with trifluoroacetate routes. (AU) | |
| FAPESP's process: | 16/12390-6 - Macro and mesoscopic superconductivity: synthesis of ceramic materials and computational simulations based on the TDGL theory |
| Grantee: | Rafael Zadorosny |
| Support Opportunities: | Regular Research Grants |