Effect of calcination temperature and pressure-assisted heat treatment on the dye degradation performance of SnO2 photocatalyst obtained by a simple synthesis method

Author(s)

da Trindade, Leticia Guerreiro ; Rocha, Ana Carolina Borba ; Teodoro, Vinicius ; da Silva, Vinicius Tineu ; Trench, Aline Barrios ; Cordoncillo, Eloisa ; Teodoro, Marcio Daldin ; Tebcherani, Sergio Mazurek ; Longo, Elson ; Mazzo, Tatiana Martelli

• Document type: Journal article
• Source: Materials Research Bulletin; v. 153, p. 12-pg., 2022-09-01.

Abstract

SnO2 particles were synthesized by the co-precipitation method. The effect of annealing temperature and pressure-assisted heat treatment (PAHT) on their structural, morphological and optical properties were investigated. Moreover, the synthetized SnO2 at ambient temperature and annealed at 400 and 700 C as well as the particles submitted at the PAHT were efficient for the photocatalytic degradation of the Rhodamine B (RhB) dye solution under UV irradiation, showing a degradation efficiency above 99% for all samples studied. However, the SnO2 sample obtained at ambient temperature (AT-SnO2) exhibited complete RhB photodegradation in only 10 min. This surprising performance of the AT-SnO2 sample led to the investigation of its performance for the degradation of two other dyes, methylene blue (MB) and methyl orange (MO), and the results also revealed complete degradation of these dyes. These findings were superior to those found in the literature for SnO2 samples synthesized by different methods. (AU)

• FAPESP's process: 13/07296-2 - CDMF - Center for the Development of Functional Materials
• Grantee: Elson Longo da Silva
• Support Opportunities: Research Grants - Research, Innovation and Dissemination Centers - RIDC