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Improving the Electrocatalytic Activities and CO Tolerance of Pt NPs by Incorporating TiO2 Nanocubes onto Carbon Supports

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Author(s):
Antoniassi, Rodolfo M. ; Quiroz, Jhon ; Barbosa, Eduardo C. M. ; Parreira, Luanna S. ; Isidoro, Roberta A. ; Spinace, Estevam, V ; Silva, Julio C. M. ; Camargo, Pedro H. C.
Total Authors: 8
Document type: Journal article
Source: CHEMCATCHEM; v. 13, n. 8, p. 9-pg., 2021-02-18.
Abstract

Designing efficient anode CO-tolerant electrocatalysts is critical in low-temperature fuel cell catalysts fueled either by H-2/CO or alcohol. We demonstrate that the incorporation of TiO2 nanocubes (TiO2NCs) on Carbon Vulcan supports, followed by the synthesis of Pt NPs at their surface (Pt/TiO2NCs-C material), led to improvements in performance towards the electrooxidation of carbon monoxide, ethanol, methanol, ethylene glycol, and glycerol in acidic media relative to the commercial Pt/C and Pt/TiO2-C counterparts employing commercial TiO2. The nanocubes enabled changes in the electronic properties of Pt NPs while contributing to the bifunctional mechanism as compared to Pt/C and Pt/TiO2-C with commercial TiO2. Fuel cell experiments fed with H-2/CO steam showed that Pt/TiO2NCs-C employing nanocubes was resistant to CO-poisoning, yielding superior performance in operational conditions. The results reported herein have important implications for developing electrocatalysts with superior performances in PEMFCs. (AU)

FAPESP's process: 15/26308-7 - Optimization of the physicochemical properties of nano -structured materials for applications in molecular recognition, catalysis and energy conversion/storage
Grantee:Roberto Manuel Torresi
Support Opportunities: Research Projects - Thematic Grants
FAPESP's process: 15/11452-5 - Hybrid materials composed of oxides and metallic nanoparticles for catalytic and photocatalytic applications
Grantee:Eduardo César Melo Barbosa
Support Opportunities: Scholarships in Brazil - Doctorate (Direct)
FAPESP's process: 14/09087-4 - Studies on the use of bioethanol in proton exchange membrane and solid oxide fuel cells
Grantee:Marcelo Linardi
Support Opportunities: Research Projects - Thematic Grants
FAPESP's process: 17/11937-4 - A sustainable path to methane conversion by advanced electrochemical technologies
Grantee:Fabio Coral Fonseca
Support Opportunities: Research Grants - Applied Research Centers Program
FAPESP's process: 16/00819-8 - Controlled Synthesis of Nanomaterials based on Pd and Pt: Electrocatalytic Activity and Stability
Grantee:Luanna Silveira Parreira
Support Opportunities: Scholarships in Brazil - Post-Doctoral
FAPESP's process: 16/17866-9 - Tailoring the catalytic properties of plasmonic Nanorattles towards the photochemical activation of oxygen under mild conditions
Grantee:Jhon Jhon Quiroz Torres
Support Opportunities: Scholarships in Brazil - Post-Doctoral
FAPESP's process: 17/15469-5 - Preparation of nanocatalysts with controlled morphology for applications in hydrogen purification and oxidation of contaminated hydrogen for electric energy generation
Grantee:Rodolfo Molina Antoniassi
Support Opportunities: Scholarships in Brazil - Post-Doctoral