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(Reference retrieved automatically from Web of Science through information on FAPESP grant and its corresponding number as mentioned in the publication by the authors.)

High-efficient microwave synthesis and characterisation of SrSnO3

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Author(s):
Bohnemann, Joerg [1, 2] ; Libanori, Rafael [1] ; Moreira, Mario L. [1] ; Longo, Elson [3]
Total Authors: 4
Affiliation:
[1] Univ Fed Sao Carlos, LIEC, BR-13565905 Sao Carlos, SP - Brazil
[2] Univ Munster, Dept Chem, D-48149 Munster - Germany
[3] Univ Estadual Paulista, Inst Quim, LIEC, BR-14800900 Araraquara, SP - Brazil
Total Affiliations: 3
Document type: Journal article
Source: CHEMICAL ENGINEERING JOURNAL; v. 155, n. 3, p. 905-909, DEC 15 2009.
Web of Science Citations: 26
Abstract

Strontium stannate (SrSnO(3)) nanostructures were obtained by microwave- assisted calcination of a SrSn(OH)(6) precursor powder. Compared to other conventional calcination methods mentioned in the literature, this procedure led to a remarkable decrease of the reaction time and the synthesis temperature owing to direct interaction of radiation with the material. X-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM) and photoluminescence measurements were performed. A comparison of the characterisation results obtained by microwave and conventional methods was conducted, and differences concerning the properties of conventionally high-temperature calcined SrSnO(3) from that obtained by microwave-assisted calcination were observed. Furthermore, two different morphologies (nanosticks and nanobrushes) were obtained by a variation of the concentration of the reactants. (C) 2009 Elsevier B.V. All rights reserved. (AU)

FAPESP's process: 98/14324-0 - Multidisciplinary Center for Development of Ceramic Materials
Grantee:Elson Longo da Silva
Support type: Research Grants - Research, Innovation and Dissemination Centers - RIDC