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(Reference retrieved automatically from SciELO through information on FAPESP grant and its corresponding number as mentioned in the publication by the authors.)

Thermal treatment effect on the microstructure, turbostraticity, and surface of reticulated vitreous carbon analyzed by xps, Raman scattering, and cyclic voltammetry

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Author(s):
Emerson Sarmento Gonçalves [1] ; Mirabel Cerqueira Rezende [2] ; Maurício Ribeiro Baldan [3] ; Neidenêi Gomes Ferreira [4]
Total Authors: 4
Affiliation:
[1] Instituto de Aeronáutica e Espaço. Centro Técnico Aeroespacial. Divisão de Materiais - Brasil
[2] Instituto de Aeronáutica e Espaço. Centro Técnico Aeroespacial. Divisão de Materiais - Brasil
[3] Instituto Nacional de Pesquisas Espaciais. Centro de Tecnologias Especiais - Brasil
[4] Instituto Nacional de Pesquisas Espaciais. Centro de Tecnologias Especiais - Brasil
Total Affiliations: 4
Document type: Journal article
Source: Química Nova; v. 32, n. 1, p. 158-164, 2009-00-00.
Abstract

The structural and surface properties of reticulated vitreous carbon (RVC) were discussed as a function of its heat treatment temperature (HTT), for samples produced in the range from 700 to 2000 ºC, using the furfuryl precursor resin. The samples were analyzed by x-ray photoelectron spectroscopy, first and second order Raman scattering as well as electrochemical response. Exploring the material turbostraticity concept, the interdependence between the RVC chemical surface variation and its defects were demonstrated. The influence of heteroatom presence was discussed in the material ordering for HTT lower than 1300 ºC while the graphitization process evolution was also pointed out for HTT higher than 1500 ºC. (AU)