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Synthesis, characterization and thermoanalytical study of lanthanum (III), lanthanides (III) and yttrium (III) with 2-methoxycinnamilidenepiruvate

Grant number: 06/06951-3
Support Opportunities:Regular Research Grants
Duration: June 01, 2008 - May 31, 2010
Field of knowledge:Physical Sciences and Mathematics - Chemistry - Analytical Chemistry
Principal Investigator:Massao Ionashiro
Grantee:Massao Ionashiro
Host Institution: Instituto de Química (IQ). Universidade Estadual Paulista (UNESP). Campus de Araraquara. Araraquara , SP, Brazil


The present research project is the synthesis of 2-methoxycinamilidenepiruvate of sodium and trivalent lantanides in the solid state. These compounds will be characterized by using infrared spectroscopy, X-ray diffractometry, elemental analysis, EDTA complexometry and the investigation of thermal behaviour by using simultaneous thermogravimetry, differential thermal analysis(TG-DTA)coupled with infrared spectroscopy and differential scanning calorimetry - Microscopy. (AU)

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Scientific publications (5)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
DE SOUZA, ADRIAN SANTOS; EKAWA, BRUNO; DE CARVALHO, CLAUDIO TEODORO; TEIXEIRA, JOSE AUGUSTO; IONASHIRO, MASSAO; DENCK COLMAN, TIAGO ANDRE. Synthesis, characterization, and thermoanalytical study of aceclofenac of light lanthanides in the solid state (La, Ce, Pr, and Nd). Thermochimica Acta, v. 683, . (13/09022-7, 06/06951-3)
DOBIES NAVIA, MARCOS VINICIUS; GALICO, DIOGO ALVES; CAIRES, FLAVIO JUNIOR; LUIZ, JOSE MARQUES; NUNES, RONALDO SPEZIA. Synthesis, thermal behavior, and spectroscopic study of the solid nalidixate of selected light trivalent lanthanides. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, v. 132, n. 3, p. 1717-1727, . (06/06951-3)
BANNACH, G.; ARCARO, R.; FERRONI, D. C.; SIQUEIRA, A. B.; TREU-FILHO, O.; IONASHIRO, M.; SCHNITZLER, E.. Thermoanalytical study of some anti-inflammatory analgesic agents. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, v. 102, n. 1, p. 163-170, . (06/06951-3)
FERRARETTO, ANA CLARA; NUNES, RONALDO SPEZIA; LUIZ, JOSE MARQUES; CAIRES, FLAVIO JUNIOR; TREU-FILHO, OSWALDO; IONASHIRO, MASSAO. Synthesis, characterization, thermal behavior, and DFT calculation of solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of some trivalent lanthanides. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, v. 118, n. 1, p. 499-509, . (06/06951-3)
BANNACH, GILBERT; CERVINI, PRISCILA; GOMES CAVALHEIRO, EDER TADEU; IONASHIRO, MASSAO. Using thermal and spectroscopic data to investigate the thermal behavior of epinephrine. Thermochimica Acta, v. 499, n. 1-2, p. 123-127, . (08/04296-3, 06/06951-3)

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