Silica infiltrated zirconia obtained through the sol-gel method for dental applications

• Grant number: 16/07920-6
• Support Opportunities: Regular Research Grants
• Start date: October 01, 2016
• End date: October 31, 2018
• Field of knowledge: Health Sciences - Dentistry - Dental Materials
• Principal Investigator: Renata Marques de Melo Marinho
• Grantee: Renata Marques de Melo Marinho
• Host Institution: Instituto de Ciência e Tecnologia (ICT). Universidade Estadual Paulista (UNESP). Campus de São José dos Campos. São José dos Campos , SP, Brazil
• Associated researchers: Tiago Moreira Bastos Campos

Abstract

Silica infiltration of zirconia used for biomedical application has already been proved to prevent low temperature degradation. In the present study, we will investigate the mechanical and bonding properties (to resin cements and porcelain) of a zirconia infiltrated by silica using a sol-gel method, which has the benefits of being simple, low-cost and cold process.Lately, zirconia infiltration occurs after five day immersion in silica sol and water. In the present work a decrease of 95.5% of the infiltration time is proposed. Therefore, the flexural strength of specimens infiltrated at several times will be measured. The structural homogeneity of the new materials will be quantified by Weibull analysis (95% CI). Microstructure will be characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD) and Fourier Transform Infrared Spectra (FTIR). Additionally, the resistance to scratching (bonding) of veneered specimens, the fracture energy of resin bonded interfaces and the resistance to wear will be measured on infiltrated zirconia. (AU)

Scientific publications

(8)

(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)

RAMOS, N. C.; ALVES, L. M. M.; RICCO, P.; SANTOS, G. M. A. S.; BOTTINO, M. A.; CAMPOS, T. M. B.; MELO, R. M.. Strength and bondability of a dental Y-TZP after silica sol-gel infiltrations. CERAMICS INTERNATIONAL, v. 46, n. 10, B, p. 17018-17024, JUL 2020. (15/16387-7, 16/07920-6, 16/20001-0)

TOYAMA, DOMINIQUE YUKIE; MARTINS ALVES, LARISSA MARCIA; RAMOS, GABRIELA FREITAS; BASTOS CAMPOS, TIAGO MOREIRA; DE VASCONCELOS, GETULIO; SOUTO BORGES, ALEXANDRE LUIZ; DE MELO, RENATA MARQUES. Bioinspired silica-infiltrated zirconia bilayers: Strength and interfacial bonding. JOURNAL OF THE MECHANICAL BEHAVIOR OF BIOMEDICAL MATERIALS, v. 89, p. 143-149, JAN 2019. (16/07920-6)

DINIZ, VANDEBERG; MONTEIRO, JAIANE BANDOLI; MEIRELES RODRIGUES, JONAS VINICIUS; CONDE OLIVEIRA PRADO, PEDRO HENRIQUE; DE MELO, RENATA MARQUES. Impact of Acid Concentration and Firing on the Long-term Bond Strength of a Zirconia-Lithium Silicate Ceramic Following Adhesive Cementation. Journal of Adhesive Dentistry, v. 21, n. 4, p. 355-363, JUL-AUG 2019. (16/07920-6)

NUNES E REIS, ANA FLAVIA; RAMOS, GABRIELA FREITAS; BASTOS CAMPOS, TIAGO MOREIRA; CONDE OLIVEIRA PRADO, PEDRO HENRIQUE; VASCONCELOS, GETULIO; SOUTO BORGES, ALEXANDRE LUIZ; DE MELO, RENATA MARQUES. The performance of sol-gel silica coated Y-TZP for veneered and monolithic dental restorations. JOURNAL OF THE MECHANICAL BEHAVIOR OF BIOMEDICAL MATERIALS, v. 90, p. 515-522, FEB 2019. (16/07920-6)

MARTINS ALVES, LARISSA MARCIA; RODRIGUES, CAMILA DA SILVA; RAMOS, GABRIELA FREITAS; BASTOS CAMPOS, TIAGO MOREIRA; DE MELO, RENATA MARQUES. ear behavior of silica-infiltrated monolithic zirconia: Effects on the mechanical properties and surface characterizatio. CERAMICS INTERNATIONAL, v. 48, n. 5, p. 6649-6656, MAR 1 2022. (18/22627-9, 17/20633-9, 16/07920-6, 15/11405-7)

RAMOS, N. C.; ALVES, L. M. M.; RICCO, P.; SANTOS, G. M. A. S.; BOTTINO, M. A.; CAMPOS, T. M. B.; MELO, R. M.. Strength and bondability of a dental Y-TZP after silica sol-gel infiltrations. CERAMICS INTERNATIONAL, v. 46, n. 10, p. 7-pg., 2020-07-01. (16/20001-0, 15/16387-7, 16/07920-6)

RAMOS, N. C.; KAIZER, M. R.; CAMPOS, T. M. B.; KIM, J.; ZHANG, Y.; MELO, R. M.. Silica-Based Infiltrations for Enhanced Zirconia-Resin Interface Toughness. JOURNAL OF DENTAL RESEARCH, v. 98, n. 4, p. 423-429, APR 2019. (16/07920-6, 16/20001-0, 15/16387-7)

CAMPOS, T. M. B.; RAMOS, N. C.; MATOS, J. D. M.; THIM, G. P.; SOUZA, R. O. A.; BOTTINO, M. A.; VALANDRO, L. F.; MELO, R. M.. Silica infiltration in partially stabilized zirconia: Effect of hydrothermal aging on mechanical properties. JOURNAL OF THE MECHANICAL BEHAVIOR OF BIOMEDICAL MATERIALS, v. 109, SEP 2020. (16/07920-6)