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Laser-Induced Breakdown Spectroscopy (LIBS) application in the analyses of electronic waste (printed circuit boards and polymers), food and difficult preparation liquid samples

Grant number: 16/01513-0
Support type:Regular Research Grants
Duration: August 01, 2017 - July 31, 2019
Field of knowledge:Physical Sciences and Mathematics - Chemistry
Principal Investigator:Edenir Rodrigues Pereira Filho
Grantee:Edenir Rodrigues Pereira Filho
Home Institution: Centro de Ciências Exatas e de Tecnologia (CCET). Universidade Federal de São Carlos (UFSCAR). São Carlos , SP, Brazil

Abstract

This research project aims at combining the results obtained by inductively coupled optical emission spectrometry (ICP OES) and laser-induced breakdown spectroscopy (LIBS) for the analysis of various types of samples, such as electronic waste (batteries, polymers and electronic circuits) food (juices and fortified food), mineral supplements and also liquid samples that are difficult to prepare (oil and honey, for example). These samples have environmental and agro-industrial importance and the results will bring new information about their composition, as well as the generation methods with minimal or no sample preparation. In addition, chemometric tools for better understanding of the results and data processing will be used. (AU)

Scientific publications (31)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
GAMELA, RAIMUNDO R.; COSTA, VINICIUS C.; SPERANCA, MARCO A.; PEREIRA-FILHO, EDENIR R. Laser-induced breakdown spectroscopy (LIBS) and wavelength dispersive X-ray fluorescence (WDXRF) data fusion to predict the concentration of K, Mg and P in bean seed samples. Food Research International, v. 132, JUN 2020. Web of Science Citations: 0.
COSTA, VINICIUS CAMARA; PEREIRA, FABIOLA MANHAS VERBI. Laser-induced breakdown spectroscopy applied to the rapid identification of different types of polyethylene used for toy manufacturing. JOURNAL OF CHEMOMETRICS, APR 2020. Web of Science Citations: 0.
ANDRADE, DANIEL FERNANDES; PEREIRA-FILHO, EDENIR RODRIGUES; AMARASIRIWARDENA, DULASIRI. Current trends in laser-induced breakdown spectroscopy: a tutorial review. APPLIED SPECTROSCOPY REVIEWS, MAR 2020. Web of Science Citations: 0.
CASTRO, JEYNE PRICYLLA; BABOS, DIEGO VICTOR; PEREIRA-FILHO, EDENIR RODRIGUES. Calibration strategies for the direct determination of rare earth elements in hard disk magnets using laser-induced breakdown spectroscopy. Talanta, v. 208, FEB 1 2020. Web of Science Citations: 0.
CASTRO, JEYNE PRICYLLA; SPERANCA, MARCO AURELIO; BABOS, DIEGO VICTOR; ANDRADE, DANIEL FERNANDES; PEREIRA-FILHO, EDENIR RODRIGUES. Neodymium determination in hard drive disks magnets using different calibration approaches for wavelength dispersive X-ray fluorescence. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v. 164, FEB 2020. Web of Science Citations: 0.
MACHADO, RAQUEL C.; ANDRADE, DANIEL F.; BABOS, V, DIEGO; CASTRO, JEYNE P.; COSTA, VINICIUS C.; SPERANCA, MARCO AURELIO; GARCIA, JOSE AUGUSTO; GAMELA, RAIMUNDO R.; PEREIRA-FILHO, EDENIR R. Solid sampling: advantages and challenges for chemical element determination-a critical review. Journal of Analytical Atomic Spectrometry, v. 35, n. 1, p. 54-77, JAN 1 2020. Web of Science Citations: 0.
ANDRADE, DANIEL FERNANDES; MACHADO, RAQUEL CARDOSO; BACCHI, MARCIO ARRUDA; PEREIRA-FILHO, EDENIR RODRIGUES. Proposition of electronic waste as a reference material - part 1: sample preparation, characterization and chemometric evaluation. Journal of Analytical Atomic Spectrometry, v. 34, n. 12, p. 2394-2401, DEC 1 2019. Web of Science Citations: 0.
ANDRADE, DANIEL FERNANDES; MACHADO, RAQUEL CARDOSO; PEREIRA-FILHO, EDENIR RODRIGUES. Proposition of electronic waste as a reference material - part 2: homogeneity, stability, characterization, and uncertainties. Journal of Analytical Atomic Spectrometry, v. 34, n. 12, p. 2402-2410, DEC 1 2019. Web of Science Citations: 0.
GAMELA, RAIMUNDO R.; SPERANCA, MARCO A.; ANDRADE, DANIEL F.; PEREIRA FILHO, EDENIR R. Hyperspectral images: a qualitative approach to evaluate the chemical profile distribution of Ca, K, Mg, Na and P in edible seeds employing laser-induced breakdown spectroscopy. ANALYTICAL METHODS, v. 11, n. 43, p. 5543-5552, NOV 21 2019. Web of Science Citations: 1.
COSTA, VINICIUS C.; PINHEIRO, FERNANDA C.; AMORIM, FABIO ALAN C.; PARANHOS DA SILVA, ERIK G.; PEREIRA-FILHO, EDENIR R. Multivariate optimization for the development of a sample preparation procedure and evaluation of calibration strategies for nutrient elements determination in handmade chocolate. Microchemical Journal, v. 150, NOV 2019. Web of Science Citations: 0.
ANDRADE, DANIEL FERNANDES; FORTUNATO, FELIPE MANFROI; PEREIRA-FILHO, EDENIR RODRIGUES. Calibration strategies for determination of the In content in discarded liquid crystal displays (LCD) from mobile phones using laser-induced breakdown spectroscopy (LIBS). Analytica Chimica Acta, v. 1061, p. 42-49, JUL 11 2019. Web of Science Citations: 6.
ANDRADE, DANIEL FERNANDES; ROMANELLI, JOAO PAULO; PEREIRA-FILHO, EDENIR RODRIGUES. Past and emerging topics related to electronic waste management: top countries, trends, and perspectives. Environmental Science and Pollution Research, v. 26, n. 17, p. 17135-17151, JUN 2019. Web of Science Citations: 2.
BABOS, DIEGO VICTOR; COSTA, VINICIUS CAMARA; PEREIRA-FILHO, EDENIR RODRIGUES. Wavelength dispersive X-ray fluorescence (WD-XRF) applied to speciation of sulphur in mineral supplement for cattle: Evaluation of the chemical and matrix effects. Microchemical Journal, v. 147, p. 628-634, JUN 2019. Web of Science Citations: 2.
ALEXANDRINA, EDUARDO CARLOS; BABOS, DIEGO VICTOR; ANDRADE, DANIEL FERNANDES; COSTA, VINICIUS CAMARA; LUI, ELAINE SCHORNOBAY; CORREA, NIVALDO APARECIDO; AGUIAR, MONICA LOPES; PEREIRA-FILHO, EDENIR RODRIGUES. Particulate matter (PM10) from Sao Carlos-SP (Brazil): spectroanalytical techniques to evaluate and determine chemical elements. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, v. 99, n. 7 MAY 2019. Web of Science Citations: 0.
BABOS, DIEGO VICTOR; BARROS, ARIANE ISIS; NOBREGA, JOAQUIM ARAUJO; PEREIRA-FILHO, EDENIR RODRIGUES. Calibration strategies to overcome matrix effects in laser-induced breakdown spectroscopy: Direct calcium and phosphorus determination in solid mineral supplements. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v. 155, p. 90-98, MAY 2019. Web of Science Citations: 3.
AUGUSTO, AMANDA S.; CASTRO, JEYNE P.; SPERANCA, MARCO A.; PEREIRA-FILHO, EDENIR R. Combination of Multi-Energy Calibration (MEC) and Laser-Induced Breakdown Spectroscopy (LIBS) for Dietary Supplements Analysis and Determination of Ca, Mg and K. Journal of the Brazilian Chemical Society, v. 30, n. 4, p. 804-812, APR 2019. Web of Science Citations: 5.
BABOS, DIEGO VICTOR; CASTRO, JEYNE PRICYLLA; ANDRADE, DANIEL FERNANDES; COSTA, VINICIUS CAMARA; PEREIRA-FILHO, EDENIR RODRIGUES. Determination and speciation of phosphorus in fertilizers and mineral supplements for cattle by X-ray absorption near-edge structure spectroscopy: a simple nondestructive method. ANALYTICAL METHODS, v. 11, n. 11, p. 1508-1515, MAR 21 2019. Web of Science Citations: 0.
COSTA, VINICIUS CAMARA; CARQUEIJA AMORIM, FABIO ALAN; DE BABOS, DIEGO VICTOR; PEREIRA-FILHO, EDENIR RODRIGUES. Direct determination of Ca, K, Mg, Na, P, S, Fe and Zn in bivalve mollusks by wavelength dispersive X-ray fluorescence (WDXRF) and laser-induced breakdown spectroscopy (LIBS). Food Chemistry, v. 273, n. SI, p. 91-98, FEB 1 2019. Web of Science Citations: 7.
SPERANCA, MARCO AURELIO; ANDRADE, DANIEL FERNANDES; CASTRO, JEYNE PRICYLLA; PEREIRA-FILHO, EDENIR RODRIGUES. Univariate and multivariate calibration strategies in combination with laser-induced breakdown spectroscopy (LIBS) to determine Ti on sunscreen: A different sample preparation procedure. OPTICS AND LASER TECHNOLOGY, v. 109, p. 648-653, JAN 2019. Web of Science Citations: 3.
VINICIUS C. COSTA; AMANDA S. AUGUSTO; JEYNE P. CASTRO; RAQUEL C. MACHADO; DANIEL F. ANDRADE; DIEGO V. BABOS; MARCO A. SPERANÇA; RAIMUNDO R. GAMELA; EDENIR R. PEREIRA-FILHO. LASER INDUCED-BREAKDOWN SPECTROSCOPY (LIBS): HISTÓRICO, FUNDAMENTOS, APLICAÇÕES E POTENCIALIDADES. Química Nova, v. 42, n. 5, p. 527-545, Maio 2019.
CASTRO, JEYNE PRICYLLA; PEREIRA-FILHO, EDENIR RODRIGUES. Spectroanalytical method for evaluating the technological elements composition of magnets from computer hard disks. Talanta, v. 189, p. 205-210, NOV 1 2018. Web of Science Citations: 7.
COSTA, VINICIUS CAMARA; CASTRO, JEYNE PRICYLLA; ANDRADE, DANIEL FERNANDES; BABOS, DIEGO VICTOR; GARCIA, JOSE AUGUSTO; SPERANCA, MARCO AURELIO; CATELANI, TIAGO AUGUSTO; PEREIRA-FILHO, EDENIR RODRIGUES. Laser-induced breakdown spectroscopy (LIBS) applications in the chemical analysis of waste electrical and electronic equipment (WEEE). TRAC-TRENDS IN ANALYTICAL CHEMISTRY, v. 108, p. 65-73, NOV 2018. Web of Science Citations: 15.
BABOS, DIEGO VICTOR; VIRGILIO, ALEX; COSTA, VINICIUS CAMARA; DONATI, GEORGE LUIS; PEREIRA-FILHO, EDENIR RODRIGUES. Multi-energy calibration (MEC) applied to laser-induced breakdown spectroscopy (LIBS). Journal of Analytical Atomic Spectrometry, v. 33, n. 10, p. 1753-1762, OCT 1 2018. Web of Science Citations: 14.
NEIVA, ARIANE MACIEL; SPERANCA, MARCO AURELIO; COSTA, VINICIUS CAMARA; CHAGAS JACINTO, MANUEL ANTONIO; PEREIRA-FILHO, EDENIR RODRIGUES. Determination of toxic metals in leather by wavelength dispersive X-ray fluorescence (WDXRF) and inductively coupled plasma optical emission spectrometry (ICP OES) with emphasis on chromium. ENVIRONMENTAL MONITORING AND ASSESSMENT, v. 190, n. 10 OCT 2018. Web of Science Citations: 1.
SPERANCA, MARCO AURELIO; VIRGILIO, ALEX; PEREIRA-FILHO, EDENIR RODRIGUES; BATISTA DE AQUINO, FRANCISCO WENDEL. Determination of Elemental Content in Solder Mask Samples Used in Printed Circuit Boards Using Different Spectroanalytical Techniques. Applied Spectroscopy, v. 72, n. 8, p. 1205-1214, AUG 2018. Web of Science Citations: 4.
COSTA, VINICIUS CAMARA; DE BABOS, DIEGO VICTOR; BATISTA DE AQUINO, FRANCISCO WENDEL; VIRGILIO, ALEX; CARQUEIJA AMORIM, FABIO ALAN; PEREIRA-FILHO, EDENIR RODRIGUES. Direct Determination of Ca, K and Mg in Cassava Flour Samples by Laser-Induced Breakdown Spectroscopy (LIBS). FOOD ANALYTICAL METHODS, v. 11, n. 7, SI, p. 1886-1896, JUL 2018. Web of Science Citations: 8.
NEIVA, ARIANE MACIEL; PEREIRA-FILHO, EDENIR RODRIGUES. Evaluation of the Chemical Composition of Synthetic Leather Using Spectroscopy Techniques. Applied Spectroscopy, v. 72, n. 6, p. 921-932, JUN 2018. Web of Science Citations: 1.
FIGUEIREDO, CAIO M.; CASTRO, JEYNE P.; SPERANCA, MARCO A.; FIALHO, LUCIMAR L.; NOBREGA, JOAQUIM A.; PEREIRA-FILHO, EDENIR R. Qualitative and Quantitative Chemical Investigation of Orthopedic Alloys by Combining Wet Digestion, Spectroanalytical Methods and Direct Solid Analysis. Journal of the Brazilian Chemical Society, v. 29, n. 4, p. 680-688, APR 2018. Web of Science Citations: 2.
BABOS, DIEGO VICTOR; COSTA, VINICIUS CAMARA; SPERANCA, MARCO AURELIO; PEREIRA-FILHO, EDENIR RODRIGUES. Direct determination of calcium and phosphorus in mineral supplements for cattle by wavelength dispersive X-ray fluorescence (WD-XRF). Microchemical Journal, v. 137, p. 272-276, MAR 2018. Web of Science Citations: 12.
FABÍOLA MANHAS VERBI PEREIRA; EDENIR RODRIGUES PEREIRA-FILHO. APLICAÇÃO DE PROGRAMA COMPUTACIONAL LIVRE EM PLANEJAMENTO DE EXPERIMENTOS: UM TUTORIAL. Química Nova, v. 41, n. 9, p. -, Set. 2018.
COSTA, VINICIUS CAMARA; BATISTA AQUINO, FRANCISCO WENDEL; PARANHOS, CAIO MARCIO; PEREIRA-FILHO, EDENIR RODRIGUES. Use of laser-induced breakdown spectroscopy for the determination of polycarbonate (PC) and acrylonitrile-butadiene-styrene (ABS) concentrations in PC/ABS plastics from e-waste. WASTE MANAGEMENT, v. 70, p. 212-221, DEC 2017. Web of Science Citations: 13.

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