Effect of activation mode of dual-cured resin cements on polymerization kinetics, mechanical properties, bond strength and stress generation

• Grant number: 07/01006-1
• Support Opportunities: Scholarships in Brazil - Doctorate
• Start date: July 01, 2007
• End date: July 31, 2008
• Field of knowledge: Health Sciences - Dentistry - Dental Clinics
• Principal Investigator: Luís Roberto Marcondes Martins
• Grantee: André Luís Faria e Silva
• Host Institution: Faculdade de Odontologia de Piracicaba (FOP). Universidade Estadual de Campinas (UNICAMP). Piracicaba , SP, Brazil

Abstract

The aim of this study will be to evaluate the influence of the light-curing and the moment when this is carried on the kinetic and degree conversion, mechanical properties, bond strength and stress generation of three dual-cured resin cements. The methodology of this study will be divided in five parts: kinetic and degree of conversion, flexural strength and elasticity modulus, bonding test, ultimate tensile strength and stress of polymerization shrinkage. The resin cements that will be evaluated are Panavia F, RelyX ARC and Enforce. The modes of activation will be: chemical activation alone, immediate light-curing or after five minutes of the material mixing, both carried through the composite blocks of 2 mm of thickness. The kinetics of conversion evaluation, in first ten minutes, and of the degree of conversion, after 24 hours, will be evaluated with Fourier-transformed infrared (FTIR) spectroscopy connected to an element of attenuated total reflectance (ATR). Specimens with 25x2x2mm will be used for the measurement of the flexural strength and the elasticity modulus of these cements, immediate and after 24 hours. The micro-shear test will be used to measure the bonding, immediate and after 24 hours, of cements. The ultimate tensile strength of cements and the stress generation by polymerization shrinkage will be also evaluated, this last through the photo elasticity method.

Scientific publications

(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)

FARIA-E-SILVA, A. L.; FABIAO, M. M.; ARIAS, V. G.; MARTINS, L. R. M.. Activation Mode Effects on the Shear Bond Strength of Dual-cured Resin Cements. Operative Dentistry, v. 35, n. 5, p. 515-521, SEP-OCT 2010. (07/01006-1, 07/00998-0)

FARIA-E-SILVA, A.; BOARO, L.; BRAGA, R.; PIVA, E.; ARIAS, V.; MARTINS, L.. Effect of Immediate or Delayed Light Activation on Curing Kinetics and Shrinkage Stress of Dual-Cure Resin Cements. Operative Dentistry, v. 36, n. 2, p. 196-204, MAR-APR 2011. (07/01006-1, 07/00998-0)

Academic Publications

(References retrieved automatically from State of São Paulo Research Institutions)

SILVA, André Luís Faria e. Effec of activation mode of dual-cured resin cements on polymerization kinetics, mechanical properties, bond strength and stress generation. 2008. Doctoral Thesis - Universidade Estadual de Campinas (UNICAMP). Faculdade de Odontologia de Piracicaba Piracicaba, SP.