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(Reference retrieved automatically from Web of Science through information on FAPESP grant and its corresponding number as mentioned in the publication by the authors.)

Thermal study of ZrO2 nanoparticles: Effect of heating and cooling cycles on solid-solid transition

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Author(s):
Gaglieri, Caroline ; Alarcon, Rafael T. ; Machado, Rafael de Godoi ; Padovini, David S. S. ; Pontes, Fenelon M. L. ; Caires, Flavio J.
Total Authors: 6
Document type: Journal article
Source: Thermochimica Acta; v. 653, p. 59-61, JUL 10 2017.
Web of Science Citations: 5
Abstract

This study investigates the influence of particle size on the solid-solid transition in zirconium (ZrO2) nanoparticles. The Simultaneous Thermogravimetry/Derivate Thermogravimetric-Differential Thermal Analysis (TG/DTG-DTA) was used to evince the phase transitions processes as well as the quantity of volatile compounds and the residual organic matter formed during the synthesis of nanoparticles. Field Emission Scanning Electron Microscopy (FE-SEM) and Transmission Electron Microscopy (TEM) were used to prove the increase and agglomeration;1;of particle size after each thermal cycle. (AU)

FAPESP's process: 12/21450-1 - Thermoanalytical studies, synthesis and characterization of the solid co-crystals of ketoprofen with some co-formers
Grantee:Gilbert Bannach
Support type: Regular Research Grants
FAPESP's process: 13/09022-7 - Thermoanalytical studies, synthesis and characterization of the solid co-crystals of antibiotics (fluoroquinolones) with some co-formers
Grantee:Massao Ionashiro
Support type: Regular Research Grants