Monitoring Electrochemical Reactions in Situ with Low Field NMR: A Mini-Review

Author(s)

Gomes, Bruna Ferreira ^[1] ; Silva Lobo, Carlos Manuel ^[1] ; Colnago, Luiz Alberto ^[2]

Affiliation

^[1] Univ Sao Paulo, Inst Quim Sao Carlos, BR-13566590 Sao Carlos, SP - Brazil

^[2] Embrapa Instrumentacao, BR-13560970 Sao Carlos, SP - Brazil

• Document type: Review article
• Source: APPLIED SCIENCES-BASEL; v. 9, n. 3 FEB 1 2019.
• Web of Science Citations: 0

Abstract

The number of applications of time domain NMR using low-field spectrometers in research and development has been steadily increasing in recent years with applications ranging from quality control of industrial products to the study of physical and chemical properties of a wide array of solid and liquid samples to, most recently, electrochemical studies. In this mini-review we summarize the progress that has been achieved in the coupling between time domain NMR (using low-field spectrometers) and electrochemistry and how the challenges that this coupling poses have been overcome over the years. We also highlight the effect that the static magnetic field of the NMR spectrometer has on the electrochemical systems. (AU)

• FAPESP's process: 16/01537-6 - Study of the coupling between electrochemistry and low-field, mid-resolution NMR for the in situ and on line analysis of redox reactions of organic compounds and the evaluation of the magnetic field effect on the velocity of the in situ reactions
• Grantee: Bruna Ferreira Gomes Lobo
• Support Opportunities: Scholarships abroad - Research Internship - Doctorate (Direct)
• FAPESP's process: 17/12864-0 - Effect of NMR magnetic field in chemical reactions monitored NMR in situ
• Grantee: Luiz Alberto Colnago
• Support Opportunities: Regular Research Grants
• FAPESP's process: 12/22281-9 - NMR study of the magneto-convective phenomenon on paramagnetic ions during electrodeposition
• Grantee: Bruna Ferreira Gomes Lobo
• Support Opportunities: Scholarships in Brazil - Doctorate (Direct)