Recent advances and future trends in new materials for sample preparation

Author(s)

Fumes, Bruno Henrique ; Silva, Meire Ribeiro ; Andrade, Felipe Nascimento ; Domingues Nazario, Carlos Eduardo ; Lancas, Fernando Mauro

• Document type: Journal article
• Source: TRAC-TRENDS IN ANALYTICAL CHEMISTRY; v. 71, p. 17-pg., 2015-09-01.

Abstract

The analysis of chemical compounds present at very low concentrations in complex matrices (e.g., residues and contaminants in food samples) usually requires a complex analytical approach, involving sampling, sample preparation, analyte isolation and qualitative and quantitative determination. Most analysts consider sample preparation to be the Achilles' heel, because it is usually time consuming, presents low yields, is prone to introducing contamination, and is more difficult to automate than other steps. Recently, a strong movement towards utilization of greener analytical methods stimulated development of microextraction techniques. Most of these microextraction techniques are based upon sorption processes, making the development of novel sorptive materials one of the most active research areas in this field. In the present work, we present a review on the new materials recently developed for sample preparation in line with the concept of green analytical chemistry. We also review the techniques using them and their main applications. (C) 2015 Elsevier B.V. All rights reserved. (AU)

• FAPESP's process: 14/07347-9 - Development of novel materials and devices for miniaturized sample preparation techniques in the area of food safety
• Grantee: Fernando Mauro Lanças
• Support Opportunities: Regular Research Grants
• FAPESP's process: 12/22055-9 - Development of silica modified with ionic liquids and their use in sample preparation techniques
• Grantee: Meire Ribeiro da Silva
• Support Opportunities: Scholarships in Brazil - Doctorate
• FAPESP's process: 13/17425-4 - Evaluation of MEPS technique applied in pesticides analysis in sugarcane juice by GC-MS
• Grantee: Bruno Henrique Fumes
• Support Opportunities: Scholarships in Brazil - Master
• FAPESP's process: 11/09898-4 - Development of molecularly imprinted polymer and use for the sample preparation and analysis of triazine and sulfonylurea in maize using high performance liquid chromatography (HPLC).
• Grantee: Felipe Nascimento Andrade
• Support Opportunities: Scholarships in Brazil - Doctorate