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(Reference retrieved automatically from SciELO through information on FAPESP grant and its corresponding number as mentioned in the publication by the authors.)

Microwave sintering of ceramics. Part III: Sintering of zirconia, mullite and alumina

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Author(s):
R. R. Menezes [1] ; P. M. Souto [2] ; R. H. G. A. Kiminami [3]
Total Authors: 3
Affiliation:
[1] Universidade Federal de S. Carlos. Departamento de Engenharia de Materiais. Laboratório de Desenvolvimento e Processamento de Materiais em Microondas - LaDProM
[2] Universidade Federal de S. Carlos. Departamento de Engenharia de Materiais. Laboratório de Desenvolvimento e Processamento de Materiais em Microondas - LaDProM
[3] Universidade Federal de S. Carlos. Departamento de Engenharia de Materiais. Laboratório de Desenvolvimento e Processamento de Materiais em Microondas - LaDProM
Total Affiliations: 3
Document type: Journal article
Source: Cerâmica; v. 53, n. 327, p. 218-226, 2007-09-00.
Abstract

Thermal processing by microwaves offers several advantages over conventional heating methods, such as shorter processing times, energy savings and improved microstructural homogeneity of ceramic bodies. Thus, this work focused on the fast hybrid microwave sintering of ceramic materials that require high sintering temperatures for densification. The materials studied here were zirconia, which displays abrupt and severe increases in dielectric loss with rising temperature, and alumina and mullite, which show low dielectric losses at ambient temperature and are difficult to microwave at low temperatures. A susceptor was used as an auxiliary heating agent. The results indicate that the sintering system developed here can be used efficiently for the rapid, homogeneous sintering of all the ceramics in question. Zirconia was sintered in 20 min, mullite in 16 min and alumina in 40 min heating cycles. (AU)