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Vibrational spectroscopy with spatial resolution

Grant number: 16/21070-5
Support type:Research Projects - Thematic Grants
Duration: April 01, 2018 - March 31, 2023
Field of knowledge:Physical Sciences and Mathematics - Chemistry - Physical-Chemistry
Principal researcher:Mauro Carlos Costa Ribeiro
Grantee:Mauro Carlos Costa Ribeiro
Home Institution: Instituto de Química (IQ). Universidade de São Paulo (USP). São Paulo , SP, Brazil
Pesquisadores principais:
Dalva Lucia Araujo de Faria ; Marcia Laudelina Arruda Temperini ; Paola Corio ; Paulo Sergio Santos ; Rômulo Augusto Ando
Assoc. researchers:Diego Pereira dos Santos ; Rômulo Augusto Ando
Associated grant(s):18/15987-9 - Frontiers and challenges of surface enhanced Raman spectroscopy (SERS), AV.EXT
18/08917-4 - Multi-user equipment approved in grant 16/21070-5: Raman spectrometer, model MultiRam, Bruker, AP.EMU
18/08918-0 - Multi-user equipment approved in grant 16/21070-5: confocal Raman microscope, Witec, AP.EMU
18/08916-8 - Multi-user equipment approved in grant 16/21070-5: infrared spectrometer with microscope, model vertex, Bruker, AP.EMU
Associated scholarship(s):22/06398-5 - Detection and Characterization of pesticides by SERS spectroscopy, BP.IC
22/06428-1 - Inclusion complexes for characterization and detection of pesticides by SERS spectroscopy, BP.IC
21/07031-5 - Multiconfigurational Calculations in the Description of Excited States Dynamics and its Correlation with Resonance Raman Spectroscopy, BP.PD
+ associated scholarships 21/05053-1 - Phase transitions and structure of deep eutectic solvents, BP.DD
20/12054-1 - Vibrational spectroscopy and properties of deep eutectic solvents, BP.IC
20/09250-3 - Hydrogen Bonding in Ionic Liquids - Vibrational Spectroscopy and Physical Properties, BP.DR
20/06307-4 - Vibrational spectroscopy and physico-chemical properties of hypergolic ionic liquids, BP.MS
20/06766-9 - Molecular dynamics of deep eutectic solvents, BP.PD
19/21939-0 - Bimetallic anisotropic nanoparticles (Au/Pd) for the study of catalytic processes through surface enhanced Raman scattering, BP.PD
19/00207-0 - Density functional theory applyed to vibrational dynamics of crystals of ionic systems., BP.PD
19/05989-7 - SERS performance of AuNP encapsulated in alginate and chitosan templates for drugs detection, BP.IC
18/25737-0 - Porous ionic liquids for the selective capture of gases, BP.DD
19/03371-6 - Investigation of the SERS and catalytic activity of plasmonic nanostructures in the degradation of organochlorine and organophosphorus pesticides, BP.DD
18/25422-9 - Biofilm synthesis based on lichen beta glucans: study of properties and identification of its vibrational signatures, BP.PD
17/12063-8 - Non-equilibrium molecular dynamics of ionic liquids, BP.PD
17/23051-0 - Phase transitions, structure, and rheology of ionic liquids, BP.DD - associated scholarships

Abstract

Several research activities in the Laboratório de Espectroscopia Molecular, Instituto de Química, Universidade de São Paulo, LEM/IQ-USP, are related to infrared and Raman spectroscopy. Coupling of optical microscopes to infrared and Raman spectrometers provides to vibrational spectroscopy the spatial resolution of the order of micrometer or below micrometer, then combining molecular structure characterization and imaging. This work includes several research projects whose development need spectral and spatial resolutions. The work will be undertaken by a group of seven professors, and their undergraduate students, PhD students, and pos-docs, of Chemistry institutes at São Paulo and Campinas universities (USP and UNICAMP). In this work, the researches in vibrational microspectroscopy include studies on solid and fluid inclusions of the order of micrometers in natural crystals of geological interest, phase transitions and glass formation of ionic liquids under wide range of pressure and temperature, hybrid materials for absorption of gases, inorganic matrixes for modified releasing of drugs and their interface with live tissues, and degradation processes of cultural goods in the forensic area and identification of falsifications and frauds. Projects in surface enhanced Raman spectroscopy (SERS) will be undertaken aiming the understanding of fundamental issues related to the mechanism of signal intensification as well as several applications. The SERS effect relies on the morphology of colloidal nanoparticles or metallic surfaces, so that these will be studied aiming the best performance of such surfaces for new technologies. The high performance SERS systems to be studied in this project include anisotropic nanoparticles, polymers and metallic nanoparticles, and bimetallic nanoparticles. These systems will be applied for analysis of species of environmental and biological interests in the range of single molecule detection, catalytic processes, for instance, carbon dioxide hydrogenation to generate fuels, and in forensic applications. (AU)

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Scientific publications (52)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
ATAIDE, VANESSA N.; AMEKU, WILSON A.; BACIL, RAPHAEL R.; ANGNES, LUCIO; DE ARAUJO, WILLIAM R.; PAIXAO, THIAGO R. L. C.. Enhanced performance of pencil-drawn paper-based electrodes by laser-scribing treatment. RSC ADVANCES, v. 11, n. 3, p. 1644-1653, . (18/14462-0, 16/21070-5, 18/08782-1, 16/16477-9, 17/10522-5)
DE SOUZA, ICARO F. T.; PASCHOAL, VITOR H.; BERNARDINO, KALIL; LIMA, THAMIRES A.; DAEMEN, LUKE L.; Y., Z.; RIBEIRO, MAURO C. C.. Vibrational spectroscopy and molecular dynamics simulation of choline oxyanions salts. JOURNAL OF MOLECULAR LIQUIDS, v. 340, . (16/21070-5, 19/00207-0, 17/12063-8)
FERNANDES, RAFAELLA F.; PAGANOTO, GIORDANO T.; TEMPERINI, MARCIA L. A.. Non-traditional intrinsic luminescence from non-conjugated polymer dots: designing a hybrid biomaterial. Polymer Chemistry, v. 12, n. 43, . (18/25422-9, 16/21070-5)
AMEKU, WILSON A.; GONCALVES, JOSUE M.; ATAIDE, VANESSA N.; SANTOS, MAURO S. FERREIRA; GUTZ, IVANO G. R.; ARAKI, KOITI; PAIXAO, THIAGO R. L. C.. Combined Colorimetric and Electrochemical Measurement Paper-Based Device for Chemometric Proof-of-Concept Analysis of Cocaine Samples. ACS OMEGA, v. 6, n. 1, p. 594-605, . (17/10522-5, 19/16491-0, 16/21070-5, 18/08782-1)
DIEGO P. DOS SANTOS; DANIEL GRASSESCHI. NANOMATERIAIS PLASMÔNICOS: PARTE II. QUÍMICA DE COORDENAÇÃO DE SUPERFÍCIE E SUA APLICAÇÃO EM SENSORES E CATALISADORES. Química Nova, v. 43, n. 10, p. 1482-1499, . (16/21070-5)
DANIEL GRASSESCHI; DIEGO P. DOS SANTOS. NANOMATERIAIS PLASMÔNICOS: PARTE I. FUNDAMENTOS DA ESPECTROSCOPIA DE NANOPARTÍCULAS E SUA RELAÇÃO COM O EFEITO SERS. Química Nova, v. 43, n. 10, p. 1463-1481, . (16/21070-5)
DOS SANTOS, DIEGO PEREIRA. Statistical Analysis of Surface-Enhanced Raman Scattering Enhancement Distributions. Journal of Physical Chemistry C, v. 124, n. 12, p. 6811-6821, . (16/21070-5)
THIAGO S. PUGLIERI; RAUL DE O. FREITAS; FRANCISCO C. B. MAIA; DALVA L. A. DE FARIA. NANOESPECTROSCOPIA DE ABSORÇÃO DE RADIAÇÃO SÍNCROTRON NO INFRAVERMELHO PARA NANOESPECIAÇÃO DE PRODUTOS DE CORROSÃO METÁLICA. Química Nova, v. 42, n. 9, p. 1050-1055, . (12/13119-3, 11/13760-8, 16/21070-5)
DALVA L. A. DE FARIA; MARCIA L. A. TEMPERINI. HANS STAMMREICH: UM DOS PRESENTES DE HITLER. Química Nova, v. 42, n. 9, p. 991-992, . (16/21070-5)
DALVA L. A. DE FARIA. HANS STAMMREICH: UMA PERSPECTIVA HISTÓRICA. Química Nova, v. 42, n. 9, p. 993-1002, . (16/21070-5)
MARIA T. C. SANSIVIERO; CARLOS E. SAMPIETRI; MARCOS V. DA COSTA; NORMA C. CASSARES; DALVA L. A. FARIA. INVENTÁRIO DO SAPATEIRO DAMIÃO SIMÕES: UM ESTUDO FÍSICO-QUÍMICO DO DOCUMENTO MAIS ANTIGO DO ESTADO DE SÃO PAULO. Química Nova, v. 42, n. 9, p. 1104-1111, . (16/21070-5)
DE BARROS, ANERISE; SHIMIZU, FLAVIO MAKOTO; DE OLIVEIRA, CRISTINE SANTOS; SIGOLI, FERNANDO APARECIDO; DOS SANTOS, DIEGO PEREIRA; MAZALI, ITALO ODONE. Dynamic Behavior of Surface-Enhanced Raman Spectra for Rhodamine 6G Interacting with Gold Nanorods: Implication for Analyses under Wet versus Dry Conditions. ACS APPLIED NANO MATERIALS, v. 3, n. 8, p. 8138-8147, . (16/21070-5, 13/22127-2)
VILLA, JAVIER E. L.; AFONSO, MARCO A. S.; DOS SANTOS, DIEGO P.; MERCADAL, PABLO A.; CORONADO, EDUARDO A.; POPPI, RONEI J.. Colloidal gold clusters formation and chemometrics for direct SERS determination of bioanalytes in complex media. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, v. 224, . (16/21070-5)
LIMA, THAMIRES A.; RIBEIRO, MAURO C. C.. Low-frequency Raman spectra of a glass-forming ionic liquid at low temperature and high pressure. Journal of Chemical Physics, v. 150, n. 16, . (16/21070-5, 14/15049-8)
SOUZA, JULIANA S.; HIRATA, FERNANDO T. H.; CORIO, PAOLA. Microwave-assisted synthesis of bismuth vanadate nanoflowers decorated with gold nanoparticles with enhanced photocatalytic activity. JOURNAL OF NANOPARTICLE RESEARCH, v. 21, n. 2, . (16/01020-3, 17/11395-7, 16/21070-5, 17/12688-8)
LIMA, THAMIRES A.; FARIA, LUIZ F. O.; PASCHOAL, VITOR H.; RIBEIRO, MAURO C. C.. Exploring the phase diagram of the ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethanesufonyl)imide. Journal of Molecular Structure, v. 1183, p. 149-156, . (16/21070-5, 15/05803-0, 14/15049-8, 15/07516-8)
FARIA, LUIZ F. O.; NOBREGA, MARCELO M.; FALSINI, NAOMI; FANETTI, SAMUELE; TEMPERINI, MARCIA L. A.; BINI, ROBERTO; RIBEIRO, MAURO C. C.. Structure and Reactivity of the Ionic Liquid 1-Allyl-3-methylimidazolium Iodide under High Pressure. Journal of Physical Chemistry B, v. 123, n. 8, p. 1822-1830, . (16/21070-5, 15/09763-2, 12/13119-3, 15/05803-0, 14/15107-8)
AMEKU, WILSON A.; DE ARAUJO, WILLIAM R.; RANGEL, CLARA J.; ANDO, ROMULO A.; PAIXAO, THIAGO R. L. C.. Gold Nanoparticle Paper-Based Dual-Detection Device for Forensics Applications. ACS APPLIED NANO MATERIALS, v. 2, n. 9, p. 5460-5468, . (16/21070-5, 17/10522-5, 18/08782-1, 16/16477-9)
PENNA, TATIANA C.; RIBEIRO, MAURO C. C.. Vibrational frequency shift of 1-alkyl-3-methylimidazolium tetrafluoroborate ionic liquids under high pressure. JOURNAL OF MOLECULAR LIQUIDS, v. 278, p. 213-218, . (16/21070-5, 13/07741-6, 12/13119-3)
RIBEIRO, MAURO C. C.. Strong anion-anion hydrogen bond in the ionic liquid 1-ethyl-3-methylimidazolium hydrogen sulfate. JOURNAL OF MOLECULAR LIQUIDS, v. 310, . (16/21070-5)
LEPRE, LUIZ FERNANDO; COSTA GOMES, MARGARIDA; ANDO, ROMULO AUGUSTO. Probing the Reorganization of Ionic Liquids' Structure Induced by CO2 Sorption. ChemPhysChem, v. 21, n. 12, . (16/21070-5, 13/23234-7, 15/07145-0)
LEPRE, LUIZ F.; GOMES, MARGARIDA COSTA; PADUA, AGILIO A. H.; ANDO, ROMULO A.; RIBEIRO, MAURO C. C.. On the Regular Behavior of a Binary Mixture of Ionic Liquids. Journal of Physical Chemistry B, v. 123, n. 30, p. 6579-6587, . (16/21070-5)
SANTOS, JONNATAN J.; TOMA, SERGIO H.; MONEZI, NATALIA M.; ANDO, ROMULO A.; CORIO, PAOLA; ARAKI, KOITI. Selecting the Mechanism of Surface-Enhanced Raman Scattering Effect using Shell Isolated Nanoparticles and an Oxo-Triruthenium Acetate Cluster Complex. Inorganic Chemistry, v. 58, n. 15, p. 10399-10407, . (16/21070-5, 19/08641-1, 18/21489-1)
MAMIAN-LOPEZ, MONICA BENICIA; MIGUEL, RODRIGO BERNARDI; ARAKI, KOITI; TEMPERINI, MARCIA L. A.; DA COSTA FERREIRA, ANA MARIA. Multivariate probing of antitumor metal-based complexes damage on living cells through Raman imaging. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, v. 244, . (14/07841-3, 16/21070-5, 12/13119-3, 18/21489-1, 13/07937-8)
MARIN, JAYR H.; TEMPERINI, MARCIA L. A.; ANDO, ROMULO A.. SERS and resonance Raman of 5-nitroisatin on silver - The distinction between the coordination and surface complexes. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, v. 263, . (16/21070-5)
DOS SANTOS, ISABELA F. S.; TEMPERINI, MARCIA L. A.. Investigation of the correlation between chemical structure and morphology in oligoaniline microspheres produced in buffered conditions. EUROPEAN POLYMER JOURNAL, v. 122, . (16/21070-5)
PASCHOAL, VITOR H.; RIBEIRO, MAURO C. C.. Structure and dynamics of aromatic and alkyl substituted Imidazolium-based ionic liquids. JOURNAL OF MOLECULAR LIQUIDS, v. 340, . (19/00207-0, 16/21070-5)
LIMA, THAMIRES A.; PASCHOAL, VITOR H.; FREITAS, RAFAEL S.; FARIA, LUIZ F. O.; LI, ZHIXIA; TYAGI, MADHUSUDAN; RIBEIRO, MAURO C. C.. An inelastic neutron scattering, Raman, far-infrared, and molecular dynamics study of the intermolecular dynamics of two ionic liquids. Physical Chemistry Chemical Physics, v. 22, n. 16, p. 9074-9085, . (15/16191-5, 15/05803-0, 16/24241-5, 14/15049-8, 19/00207-0, 16/21070-5)
DE SOUZA, RAFAEL MAGLIA; KARTTUNEN, MIKKO; COSTA RIBEIRO, MAURO CARLOS. ine-Tuning the Polarizable CL&Pol Force Field for the Deep Eutectic Solvent Ethalin. JOURNAL OF CHEMICAL INFORMATION AND MODELING, v. 61, n. 12, p. 5938-5947, . (16/21070-5, 20/06766-9)
RODRIGUES, BARBARA SCOLA; BRANCO, CAROLYNE MARTINS; CORIO, PAOLA; SOUZA, JULIANA S.. Controlling Bismuth Vanadate Morphology and Crystalline Structure through Optimization of Microwave-Assisted Synthesis Conditions. Crystal Growth & Design, v. 20, n. 6, p. 3673-3685, . (16/21070-5, 17/11395-7, 17/26633-0, 19/26010-9)
PASCHOAL, VITOR H.; RIBEIRO, MAURO C. C.. Pseudo-Optical Modes in Room-Temperature Ionic Liquids. Journal of Physical Chemistry B, v. 124, n. 13, p. 2661-2667, . (16/21070-5, 15/07516-8, 19/00207-0)
NATÁLIA M. MONEZI; LUIZ F. LEPRE; RÔMULO A. ANDO. UNRAVELING THE SOLVATOCHROMISM OF A TRIARYLMETHANE DYE BY RESONANCE RAMAN SPECTROSCOPY. Química Nova, v. 42, n. 9, p. 1116-1121, . (16/21070-5, 13/23234-7)
MÓNICA B. MAMIÁN-LÓPEZ; MARCIA L. A. TEMPERINI. HOTSPOT STABILIZATION OF GOLD NANOPARTICLES FOR APPLICATION OF QUANTITATIVE SERS IN BIOANALYTICAL SYSTEMS. Química Nova, v. 42, n. 9, p. 1084-1090, . (16/21070-5)
DAYANE V. N. DOS SANTOS; DIEGO P. DOS SANTOS. CORRELATING SINGLE-MOLECULE SERS STATISTICS TO PLASMONIC NANOCLUSTER STRUCTURE AND NEAR-FIELD PROPERTIES. Química Nova, v. 42, n. 9, p. 1029-1037, . (16/21070-5)
BERNARDINO, KALIL; LIMA, THAMIRES A.; RIBEIRO, MAURO C. C.. Low-Temperature Phase Transitions of the Ionic Liquid 1-Ethyl-3-methylimidazolium Dicyanamide. Journal of Physical Chemistry B, v. 123, n. 44, p. 9418-9427, . (16/21070-5, 17/12063-8, 14/15049-8, 19/04785-9)
VIEIRA, EDUARDO GUIMARAES; MIGUEL, RODRIGO BERNARDI; DA SILVA, DANIEL RODRIGUES; FAZZI, RODRIGO BONI; ALVES DE COUTO, RICARDO ALEXANDRE; MARIN, JAYR HENRIQUE; ARRUDA TEMPERINI, MARCIA LAUDELINA; SHINOHARA, JORGE DA SILVA; TOMA, HENRIQUE EISI; RUSSO, LILIAN CRISTINA; et al. Functionalized nanoparticles as adjuvant to increase the cytotoxicity of metallodrugs toward tumor cells. NEW JOURNAL OF CHEMISTRY, v. 43, n. 1, p. 386-398, . (11/50318-1, 17/21919-3, 13/07937-8, 16/21070-5, 16/16735-8)
DOS SANTOS, PAMYLA L.; KATIC, VERA; LOUREIRO, HUGO C.; DOS SANTOS, MATHEUS F.; DOS SANTOS, DIEGO P.; FORMIGA, ANDRE L. B.; BONACIN, JULIANO A.. Enhanced performance of 3D printed graphene electrodes after electrochemical pre-treatment: Role of exposed graphene sheets. SENSORS AND ACTUATORS B-CHEMICAL, v. 281, p. 837-848, . (13/22127-2, 17/23960-0, 16/21070-5)
PASTORELLO, MURILO; SIGOLI, FERNANDO A.; DOS SANTOS, DIEGO P.; MAZALI, ITALO O.. On the use of Au@Ag core-shell nanorods for SERS detection of Thiram diluted solutions. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, v. 231, . (16/21070-5, 13/22127-2)
DE SOUZA, ICARO F. T.; RIBEIRO, MAURO C. C.. A Raman spectroscopy and rheology study of the phase transitions of the ionic liquid choline acetate. JOURNAL OF MOLECULAR LIQUIDS, v. 322, . (17/23051-0, 16/21070-5)
MARQUES, LEANDRO RAMOS; ANDO, ROMULO AUGUSTO. Probing the Charge Transfer in a Frustrated Lewis Pair by Resonance Raman Spectroscopy and DFT Calculations. ChemPhysChem, v. 22, n. 6, . (16/21070-5)
BERNARDINO, KALIL; ZHANG, YONG; RIBEIRO, MAURO C. C.; MAGINN, EDWARD J.. Effect of alkyl-group flexibility on the melting point of imidazolium-based ionic liquids. Journal of Chemical Physics, v. 153, n. 4, . (16/21070-5, 17/12063-8, 19/04785-9)
MORSELLI, GIOVANNI R.; ANDO, ROMULO A.. SO2 capture by tricyanomethanide ionic liquids: Unraveling anion-gas interactions by resonance Raman spectroscopy. Chemical Physics Letters, v. 784, . (16/21070-5)
BERNARDINO, KALIL; RIBEIRO, MAURO C. C.. Relating the structure and dynamics of ionic liquids under shear by means of reverse non-equilibrium molecular dynamics simulations. Physical Chemistry Chemical Physics, v. 23, n. 25, p. 13984-13995, . (19/04785-9, 17/12063-8, 16/21070-5)
DE MATOS, CAROLINE S.; NOBREGA, MARCELO M.; TEMPERINI, MARCIA L. A.; CONSTANTINO, VERA R. L.. Hybrid Ni-Al layered double hydroxide: Characterization and in situ synchrotron XRD and vibrational spectroscopic studies under high-pressure. APPLIED CLAY SCIENCE, v. 174, p. 152-158, . (16/21070-5, 11/50318-1, 15/09763-2, 14/04816-8, 14/15107-8)
SOUZA, KLESTER S.; TEIXEIRA-NETO, ERICO; TEMPERINI, MARCIA L. A.; DOS SANTOS, DIEGO P.. Interplay between Near-Field Properties and Au Nanorod Cluster Structure: Extending Hot Spots for Surface-Enhanced Raman Scattering. Journal of the Brazilian Chemical Society, v. 30, n. 12, SI, p. 2624-2633, . (16/21070-5, 11/17923-9)
DOS SANTOS, DIEGO P.; TEMPERINI, MARCIA L. A.; BROLO, ALEXANDRE G.. Intensity Fluctuations in Single-Molecule Surface-Enhanced Raman Scattering. ACCOUNTS OF CHEMICAL RESEARCH, v. 52, n. 2, p. 456-464, . (16/21070-5, 18/15987-9)
DE SOUZA, MICHELE LEMOS; DOS SANTOS, DIEGO PEREIRA; CORIO, PAOLA. Localized surface plasmon resonance enhanced photocatalysis: an experimental and theoretical mechanistic investigation. RSC ADVANCES, v. 8, n. 50, p. 28753-28762, . (16/21070-5, 08/03636-5)
BERNARDINO, KALIL; GOLOVIZNINA, KATERYNA; GOMES, MARGARIDA COSTA; PADUA, AGILIO A. H.; RIBEIRO, MAURO C. C.. Ion pair free energy surface as a probe of ionic liquid structure. Journal of Chemical Physics, v. 152, n. 1, . (16/21070-5, 17/12063-8, 19/04785-9)
BATISHCHEVA, ELIZAVETA V.; SOKOLOVA, DARYA N.; FEDOTOVA, VERONIKA S.; SOKOLOVA, MARIA P.; NIKOLAEVA, ALEXANDRA L.; VAKULYUK, ALEXEY Y.; SHAKHBAZOVA, CHRISTINA Y.; RIBEIRO, MAURO CARLOS COSTA; KARTTUNEN, MIKKO; SMIRNOV, MICHAEL A.. Strengthening Cellulose Nanopaper via Deep Eutectic Solvent and Ultrasound-Induced Surface Disordering of Nanofibers. POLYMERS, v. 14, n. 1, . (16/21070-5)
FERNANDES, RAFAELLA F.; ALVES, GUSTAVO A. S.; GONCALVES, RENATO V.; TEMPERINI, MARCIA L. A.. A Methodology to Identify the Releasing of the Amide-Containing beta-Glucan from the Usnea Lichen: A Spectroscopic Study. JOURNAL OF POLYMERS AND THE ENVIRONMENT, v. 29, n. 10, p. 3105-3115, . (18/25422-9, 16/21070-5)

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