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(Reference retrieved automatically from SciELO through information on FAPESP grant and its corresponding number as mentioned in the publication by the authors.)

Infra-red heating as an alternative technique for fast sample preparation

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Author(s):
Sandro T. Gouveia [1] ; Orlando Fatibello-Filho [2] ; Joaquim A. Nóbrega [3]
Total Authors: 3
Affiliation:
[1] Universidade Federal do Ceará. Departamento de Química Analítica e Físico-Química - Brasil
[2] Universidade Federal de São Carlos. Departamento de Química - Brasil
[3] Universidade Federal de São Carlos. Departamento de Química - Brasil
Total Affiliations: 3
Document type: Journal article
Source: Journal of the Brazilian Chemical Society; v. 11, n. 3, p. 261-265, 2000-06-00.
Abstract

A procedure for sample preparation was investigated in this work using infra-red radiation generated by tungsten lamps for fast heating of an acidic sample suspension contained in a glass flask. The main advantages of the developed procedure are its simplicity and low-cost. Additionally the dilute acid solution is heated in less than 60 s and the total sample preparation is performed in less than 5 min. The proposed procedure is suitable for trace analysis and it can be easily implemented. The preliminary investigations focus on the determination of Cu, Fe, Mn, and Zn in bovine liver and apple leaves as standard reference materials. All results are in agreement at a 95% confidence level. Copper and Mn were also determined in a sample of bovine liver without any sample pretreatment or after a freeze-drying step for comparison. For this sample, the results were validated using a conventional microwave-assisted closed vessel procedure. (AU)

FAPESP's process: 98/10814-3 - Preparation of agronomic samples and multi-elementary determination by induced plasma atomic emission spectrometry
Grantee:Joaquim de Araújo Nóbrega
Support Opportunities: Research Projects - Thematic Grants