Role of supercritical CO2 impregnation variables on ?-carotene loading into corn starch aerogel particles

Author(s)

Dias, Arthur Luiz Baiao ; Hatami, Tahmasb ; Vigano, Juliane ; de Araujo, Erick Jarles Santos ; Mei, Lucia Helena Innocentini ; Rezende, Camila Alves ; Martinez, Julian

• Document type: Journal article
• Source: JOURNAL OF CO2 UTILIZATION; v. 63, p. 11-pg., 2022-07-08.

Abstract

beta-carotene is a natural dye with antioxidant and provitamin A activities, which has essential roles in human health. However, its direct use in food products is unviable since it is susceptible to oxidation, easily isomerization under light, heat or acids, and has low water solubility and oral bioavailability. To address this issue, this work reports, for the first time, the impregnation of beta-carotene into corn starch aerogels using supercritical carbon dioxide (sc-CO2). The aerogel particles were produced by the emulsion-gelation method, dried by sc-CO2 and loaded with beta-carotene by sc-CO2 impregnation. The impacts of pressure (15 and 30 MPa), temperature (40 and 60 degrees C), average depressurization rate (0.25-2.61 MPa/min), and cycles (1-4) were investigated on loading. Excepting depressurization rate, all variables played fundamental roles in loading, reaching a maximum of 0.96 mg beta-carotene/g aerogel (30 MPa, 40 degrees C, 0.40 MPa/min, four cycles). (AU)

• FAPESP's process: 20/15774-5 - Development of methods of extraction, separation and two-dimensional analysis of phenolic compounds in natural products
• Grantee: Juliane Viganó
• Support Opportunities: Scholarships in Brazil - Post-Doctoral
• FAPESP's process: 18/23769-1 - Preparation and applications of nanostructures from plant biomass
• Grantee: Camila Alves de Rezende
• Support Opportunities: Regular Research Grants
• FAPESP's process: 18/18722-6 - Constructing a supercritical deposition-foaming unit for 3D supports (scaffold) fabrication: Experiment, mathematical modeling, and optimization
• Grantee: Tahmasb Hatami
• Support Opportunities: Scholarships in Brazil - Post-Doctoral