Multi-User Equipment aproved in grant 2013/09543-7: ultra high performance liquid chromatography with photodiode array detector and Fluorescence Detector (UPLC-DAD-FLD)

• Grant number: 14/06064-3
• Support Opportunities: Multi-user Equipment Program
• Start date: June 01, 2014
• End date: May 31, 2016
• Field of knowledge: Physical Sciences and Mathematics - Chemistry - Analytical Chemistry
• Principal Investigator: Susanne Rath
• Grantee: Susanne Rath
• Host Institution: Instituto de Química (IQ). Universidade Estadual de Campinas (UNICAMP). Campinas , SP, Brazil
• City of the host institution: Campinas
• Associated research grant: 13/09543-7 - Residues of veterinary drugs in the environment, AP.TEM
• EMU web page: Página do Equipamento Multiusuário não informada
• Type of equipment: Caracterização de Materiais - Análises Químicas - Cromatrografia líquida
• Manufacturer: Fabricante não informado
• Model: Modelo não informado

Abstract

This Multi-equipment project aims the installation of an Ultra High Performance Liquid Chromatograph coupled to a Photodiode Array and Fluorescencen Detector (UPLC-DAD-FLD) in an institutional space (Institute of Chemistry, UNICAMP) to attend the thematic project entitled "RESIDUES OF VETERINARY DRUGS IN THE ENVIRONMENT" (FAPESP 2013/09543-7), as well as other projects of researchers from the internal and external community of the Institute of Chemistry, UNICAMP.In recent years, ultra-high performance liquid chromatography (UHPLC) has replaced high performance liquid chromatography (HPLC) in research and industrial laboratories, since this system allows the chromatograph to work with higher efficiency in a wider range of linear velocity, flow rate and compression, leading to a higher separation efficiency combined with a gain of detectability and lower solvent consumption and analysis time. The photodiode array detectors and fluorescence in series allows the detection of a variety of molecules. Thus, the required equipment has a wide application in various areas of technological sciences, and health and technology. The analytical versatility of the equipment must meet the needs of many research groups and specially the research group of the tematic project which aims to evaluate the environmental impact of veterinary drugs in the environment. (AU)

Scientific publications

(4)

(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)

CAIANELO, MARLON; RODRIGUES-SILVA, CAIO; MANIERO, MILENA GUEDES; GUIMARAES, JOSE ROBERTO. Antimicrobial activity against Gram-positive and Gram-negative bacteria during gatifloxacin degradation by hydroxyl radicals. Environmental Science and Pollution Research, v. 24, n. 7, p. 6288-6298, MAR 2017. (14/16622-3, 14/06064-3, 13/09543-7, 13/04656-8, 13/07817-2, 14/06201-0)

URBANO, VANESSA RIBEIRO; MANIERO, MILENA GUEDES; PEREZ-MOYA, MONTSERRAT; GUIMARAES, JOSE ROBERTO. Influence of pH and ozone dose on sulfaquinoxaline ozonation. Journal of Environmental Management, v. 195, p. 8-pg., 2017-06-15. (14/06064-3, 13/04656-8, 13/09543-7, 14/06201-0, 13/07817-2)

URBANO, VANESSA RIBEIRO; MANIERO, MILENA GUEDES; PEREZ-MOYA, MONTSERRAT; GUIMARAES, JOSE ROBERTO. Influence of pH and ozone dose on sulfaquinoxaline ozonation. Journal of Environmental Management, v. 195, n. 2, SI, p. 224-231, JUN 15 2017. (13/04656-8, 14/06201-0, 13/07817-2, 13/09543-7, 14/06064-3)

LIMA VENANCIO, WILSON AUGUSTO; RODRIGUES-SILVA, CAIO; MANIERO, MILENA GUEDES; GUIMARAES, JOSE ROBERTO. Photocatalytic removal of fluoroquinolones and their antimicrobial activity from water matrices at trace levels: a comparison of commercial TiO2 catalysts. WATER SCIENCE AND TECHNOLOGY, v. 78, n. 8, p. 1668-1678, NOV 2018. (14/06201-0, 13/07817-2, 13/09543-7, 14/16622-3, 14/06064-3)