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Multi-User Equipment approved in grant 2015/05942-0: micro X-Ray Fluorescence system

Grant number: 15/19121-8
Support type:Multi-user Equipment Program
Duration: November 01, 2015 - October 31, 2017
Field of knowledge:Physical Sciences and Mathematics - Chemistry - Analytical Chemistry
Principal Investigator:Hudson Wallace Pereira de Carvalho
Grantee:Hudson Wallace Pereira de Carvalho
Home Institution: Centro de Energia Nuclear na Agricultura (CENA). Universidade de São Paulo (USP). Piracicaba , SP, Brazil
Associated research grant:15/05942-0 - Shedding light on the metabolism of nanomaterials absorbed by plants with X-ray and vibrational spectroscopy, AP.JP
As informações de acesso ao Equipamento Multiusuário são de responsabilidade do Pesquisador responsável
EMU web page: Página do Equipamento Multiusuário não informada
Tipo de equipamento:Caracterização de Materiais - Microscopia ótica - Fluorescência
Caracterização de Materiais - Espectroscopia - Emissão de raios-X (ICP, ICP-MS, LIBS)
Fabricante: Fabricante não informado
Modelo: Modelo não informado

Abstract

As previously discussed in the granted proposal the micro-XRF facility will be used to map the roots, steam, leaves and seeds exposed to nanomaterials. Due to space resolution offered by the micro-XRF it will be possible to trace the specialized tissues where the nanomaterials are accumulated. Besides finding out the storage hotspots, it will be possible to estimate the concentration of nanomaterials. Since micro-XRF is a multi-elemental technique, the distribution of other essential macro and micronutrients will be as well evaluated. The combination of these two maps will allow investigating how the nanomaterials influence the plant's micro-metabolism; therefore it might help to understand why some nanomaterials are toxic whereas others promote the plant's growth. The micro-XRF facility will make possible to carry out bold experiments to in vivo monitor the absorption and metabolism of nanomaterials. This equipment will still be used as a high-throughput tool for quantitative analysis using Elisa wells or pellets; this approach is especially valuable in cases which only small amounts of sample are available. Thanks to its versatility the micro-XRF can be used by scientists working in several fields of knowledge such as soil sciences, materials science and biology among many others. This technique can produce chemical images in micrometric level for rocks, biologic tissues, coatings and materials micro morphology. It is worthy highlighting that micro-XRF is non-destructive, does not require vacuum and achieves detection limits much lower than those exhibited by SEM-EDX. This multi-user facility will be shared with other research groups as described in the management plan. (AU)

Scientific publications (23)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
ANTONANGELO, JOAO A.; FIRMANO, RUAN F.; ZHANG, HAILIN; COLZATO, MARINA; ABDALA, DALTON B.; CARVALHO, HUDSON W. P.; DE OLIVEIRA JUNIOR, ADILSON; ALLEONI, LUIS R. F. Phosphorus speciation by P-XANES in an Oxisol under long-term no-till cultivation. Geoderma, v. 377, NOV 1 2020. Web of Science Citations: 0.
LOUVANDINI, HELDER; IEDA, EGON H.; JIMENEZ, CAROLINA R.; CORREA, PATRICIA SPOTO; MORETTI, DEBORA B.; LIMA, PAULO M. T.; MCMANUS, CONCEPTA M.; CARVALHO, HUDSON W. P.; FERNANDES, ELISABETE A. DE N. Effects of Maternal Dietary Cottonseed on the Profile of Minerals in the Testes of the Lamb. BIOLOGICAL TRACE ELEMENT RESEARCH, v. 197, n. 1, p. 159-166, SEP 2020. Web of Science Citations: 3.
ALMEIDA, EDUARDO DE; MONTANHA, GABRIEL SGABIERO; CARVALHO, HUDSON W. PEREIRA DE; MARGUI, EVA. Evaluation of energy dispersive X-ray fluorescence and total reflection X-ray fluorescence spectrometry for vegetal mass-limited sample analysis: Application to soybean root and shoots. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v. 170, AUG 2020. Web of Science Citations: 0.
FIRMANO, RUAN F.; MELO, VANDER FREITAS; MONTES, CELIA REGINA; DE OLIVEIRA JUNIOR, ADILSON; DE CASTRO, CESAR; FERRACCIU ALLEONI, LUS REYNALDO. POTASSIUM RESERVES IN THE CLAY FRACTION OF A TROPICAL SOIL FERTILIZED FOR THREE DECADES. CLAYS AND CLAY MINERALS, v. 68, n. 3 JUL 2020. Web of Science Citations: 1.
CARVALHO, CAROLINNE R.; DIAS, ARMANDO C. F.; HOMMA, SERGIO K.; CARDOSO, ELKE J. B. N. Phyllosphere bacterial assembly in citrus crop under conventional and ecological management. PeerJ, v. 8, JUN 2 2020. Web of Science Citations: 0.
MONTANHA, GABRIEL SGARBIERO; RODRIGUES, EDUARDO SANTOS; RODRIGUES MARQUES, JOAO PAULO; DE ALMEIDA, EDUARDO; COLZATO, MARINA; PEREIRA DE CARVALHO, HUDSON WALLACE. Zinc nanocoated seeds: an alternative to boost soybean seed germination and seedling development. SN APPLIED SCIENCES, v. 2, n. 5 MAY 2020. Web of Science Citations: 0.
RODRIGUES MARQUES, JOAO PAULO; SPOSITO, MARCEL BELLATO; AMORIM, LILIAN; MONTANHA, GABRIEL SGARBIERO; SILVA JUNIOR, GERALDO JOSE; PEREIRA DE CARVALHO, HUDSON WALLACE; APPEZZATO-DA-GLORIA, BEATRIZ. Persistent Calyxes in Postbloom Fruit Drop: A Microscopy and Microanalysis Perspective. PATHOGENS, v. 9, n. 4 APR 2020. Web of Science Citations: 0.
ORTEGA RODRIGUEZ, DAIGARD RICARDO; DE ALMEIDA, EDUARDO; TOMAZELLO-FILHO, MARIO; PEREIRA DE CARVALHO, HUDSON WALLACE. Space-resolved determination of the mineral nutrient content in tree-rings by X-ray fluorescence. Science of The Total Environment, v. 708, MAR 15 2020. Web of Science Citations: 0.
DOS REIS, ANDRE RODRIGUES; MARCANDALLI BOLETA, EDUARDO HENRIQUE; ALVES, CHARLINE ZARATIN; COTRIM, MAYARA FAVERO; BARBOSA, JULIERME ZIMMER; SILVA, VINICIUS MARTINS; PORTO, RAFAEL LAWANDOVSKI; DANTAS BERETA LANZA, MARIA GABRIELA; LAVRES, JOSE; FERESIN GOMES, MARCOS HENRIQUE; PEREIRA DE CARVALHO, HUDSON WALLACE. Selenium toxicity in upland field-grown rice: Seed physiology responses and nutrient distribution using the mu-XRF technique. ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY, v. 190, MAR 1 2020. Web of Science Citations: 0.
MONTANHA, GABRIEL S.; RODRIGUES, EDUARDO S.; ROMEU, SARA L. Z.; DE ALMEIDA, EDUARDO; REIS, ANDRE R.; LAVRES JR, JOSE; PEREIRA DE CARVALHO, HUDSON W. Zinc uptake from ZnSO4 (aq) and Zn-EDTA ((aq)) and its root-to-shoot transport in soybean plants (Glycine max) probed by time-resolved in vivo X-ray spectroscopy. Plant Science, v. 292, MAR 2020. Web of Science Citations: 1.
MONTANHA, GABRIEL SGARBIERO; RODRIGUES, EDUARDO SANTOS; MARQUES, JOAO PAULO RODRIGUES; DE ALMEIDA, EDUARDO; DOS REIS, ANDRE RODRIGUES; PEREIRA DE CARVALHO, HUDSON WALLACE. X-ray fluorescence spectroscopy (XRF) applied to plant science: challenges towards in vivo analysis of plants. METALLOMICS, v. 12, n. 2, p. 183-192, FEB 1 2020. Web of Science Citations: 0.
MOLINA, EDUARDO FERREIRA; MARTINS DE JESUS, NATANA APARECIDA; PAOFAI, SERGE; HAMMER, PETER; AMELA-CORTES, MARIA; ROBIN, MALO; CORDIER, STEPHANE; MOLARD, YANN. When a Red-NIR-Emissive Cs2[Mo6Br14] Interacts with an Active Diureasil-PEO Matrix: Design of Tunable and White-Light-Emitting Hybrid Material. CHEMISTRY-A EUROPEAN JOURNAL, v. 25, n. 67, p. 15248-15251, DEC 2 2019. Web of Science Citations: 0.
MACHADO, BIANCA A.; GOMES, MARCOS H. F.; MARQUES, JOAO P. R.; OTTO, RAFAEL; DE CARVALHO, HUDSON W. P. X-ray Spectroscopy Fostering the Understanding of Foliar Uptake and Transport of Mn by Soybean (Glycine max L. Merril): Kinetics, Chemical Speciation, and Effects of Glyphosate. Journal of Agricultural and Food Chemistry, v. 67, n. 47, p. 13010-13020, NOV 27 2019. Web of Science Citations: 0.
COTRIM, MAYARA FAVERO; DA SILVA, JOSUE BISPO; DOS SANTOS LOURENCO, FLAVIA MENDES; TEIXEIRA, ANIELLI VERZOTTO; GAVA, RICARDO; ALVES, CHARLINE ZARATIN; DA SILVA CANDIDO, ANA CARINA; SILVA CAMPOS, CID NAUDI; PEREIRA, MARCIO DIAS; TORRES, SALVADOR BARROS; BACCHETTA, GIANLUIGI; TEODORO, PAULO EDUARDO. Studying the link between physiological performance of Crotalaria ochroleuca and the distribution of Ca, P, K and S in seeds with Xray fluorescence. PLoS One, v. 14, n. 9 SEP 26 2019. Web of Science Citations: 0.
MARUCCI, ROSANGELA CRISTINA; FREITAS, LARAH MARTINS; SANTOS-RASERA, JOYCE RIBEIRO; ALVES, DEJANE SANTOS; CARVALHO, GERALDO ANDRADE; PEREIRA DE CARVALHO, HUDSON WALLACE. Are cerium oxide nanoparticles transferred from plants to the aphid Myzus perskae (Hemiptera: Aphididae)?. FLORIDA ENTOMOLOGIST, v. 102, n. 3, p. 555-561, SEP 2019. Web of Science Citations: 0.
SANTINI, LUIZ; ORTEGA RODRIGUEZ, DAIGARD RICARDO; QUINTILHAN, MANOLO TRINDADE; BRAZOLIN, SERGIO; TOMMASIELLO FILHO, MARIO. Evidence to wood biodeterioration of tropical species revealed by non-destructive techniques. Science of The Total Environment, v. 672, p. 357-369, JUL 1 2019. Web of Science Citations: 0.
FRAZAO, JOAQUIM JOSE; BENITES, VINICIUS DE MELO; SCHIAVON RIBEIRO, JOAO VICTOR; PIEROBON, VITOR MATEUS; LAVRES, JOSE. Agronomic effectiveness of a granular poultry litter-derived organomineral phosphate fertilizer in tropical soils: Soil phosphorus fractionation and plant responses. Geoderma, v. 337, p. 582-593, MAR 1 2019. Web of Science Citations: 0.
ORTEGA RODRIGUEZ, DAIGARD RICARDO; PEREIRA DE CARVALHO, HUDSON WALLACE; TOMAZELLO-FILHO, MARIO. Nutrient concentrations of 17-year-old Pinus taeda annual tree-rings analyzed by X-ray fluorescence microanalysis. DENDROCHRONOLOGIA, v. 52, p. 67-79, DEC 2018. Web of Science Citations: 2.
SAVASSA, SUSILAINE M.; DURAN, NADIA M.; RODRIGUES, EDUARDO S.; DE ALMEIDA, EDUARDO; VAN GESTEL, CORNELIS A. M.; BOMPADRE, THIAGO F. V.; DE CARVALHO, HUDSON W. P. Effects of ZnO Nanoparticles on Phaseolus vulgaris Germination and Seedling Development Determined by X-ray Spectroscopy. ACS APPLIED NANO MATERIALS, v. 1, n. 11, p. 6414-6426, NOV 2018. Web of Science Citations: 1.
DURAN, NADIA M.; MEDINA-LLAMAS, MARIA; CASSANJI, JOAO G. B.; DE LIMA, RAFAEL G.; DE ALMEIDA, EDUARDO; MACEDO, WILLIAN R.; MATTIA, DAVIDE; PEREIRA DE CARVALHO, HUDSON W. Bean Seedling Growth Enhancement Using Magnetite Nanoparticles. Journal of Agricultural and Food Chemistry, v. 66, n. 23, p. 5746-5755, JUN 13 2018. Web of Science Citations: 1.
SILVA, VINICIUS MARTINS; MARCANDALLI BOLETA, EDUARDO HENRIQUE; DANTAS BERETA LANZA, MARIA GABRIELA; LAVRES, JOSE; MARTINS, JULIANA TRINDADE; SANTOS, ELCIO FERREIRA; MENDES DOS SANTOS, FLAYIA LOURENCO; PUTTI, FERNANDO FERRARI; FURLANI JUNIOR, ENES; WHITE, PHILIP J.; BROADLEY, MARTIN R.; PEREIRA DE CARVALHO, HUDSON WALLACE; DOS REIS, ANDRE RODRIGUES. Physiological, biochemical, and ultrastructural characterization of selenium toxicity in cowpea plants. ENVIRONMENTAL AND EXPERIMENTAL BOTANY, v. 150, p. 172-182, JUN 2018. Web of Science Citations: 14.
DA CRUZ, TATIANA N. M.; SAVASSA, SUSILAINE M.; GOMES, MARCOS H. F.; RODRIGUES, EDUARDO S.; DURAN, NADIA M.; DE ALMEIDA, EDUARDO; MARTINELLI, ADRIANA P.; DE CARVALHO, HUDSON W. P. Shedding light on the mechanisms of absorption and transport of ZnO nanoparticles by plants via in vivo X-ray spectroscopy. ENVIRONMENTAL SCIENCE-NANO, v. 4, n. 12, p. 2367-2376, DEC 2017. Web of Science Citations: 10.
DURAN, NADIA M.; SAVASSA, SUSILAINE M.; DE LIMA, RAFAEL GIOVANINI; DE ALMEIDA, EDUARDO; LINHARES, FRANCISCO S.; VAN GESTEL, CORNELIS A. M.; PEREIRA DE CARVALHO, HUDSON W. X-ray Spectroscopy Uncovering the Effects of Cu Based Nanoparticle Concentration and Structure on Phaseolus vulgaris Germination and Seedling Development. Journal of Agricultural and Food Chemistry, v. 65, n. 36, p. 7874-7884, SEP 13 2017. Web of Science Citations: 8.

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