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Development of an automated system for biofuel precursor production using sub-critical technology

Grant number: 19/26925-7
Support Opportunities:Scholarships in Brazil - Doctorate (Direct)
Effective date (Start): March 01, 2020
Effective date (End): April 30, 2023
Field of knowledge:Agronomical Sciences - Food Science and Technology - Food Engineering
Principal Investigator:Tânia Forster Carneiro
Grantee:William Gustavo Sganzerla
Host Institution: Faculdade de Engenharia de Alimentos (FEA). Universidade Estadual de Campinas (UNICAMP). Campinas , SP, Brazil
Associated research grant:18/14938-4 - Waste2energy: integration of supercritical technologies and anaerobic digestion through an automated system for the production of biofuel precursors, AP.JP2
Associated scholarship(s):21/12762-9 - Subcritical water pretreatment of brewer's spent grains for bio-based products manufacturing in a biorefinery concept, BE.EP.DD

Abstract

Biomass conversion and waste reuse technologies for the production of new energy-using products are emerging, among them sub-critical technology that uses water as a solvent in a clean and sustainable process. In order to improve this technology, it is proposed to assemble an experimental unit composed of series reactors and parallel hydrolysis in subcritical water. This research and technological innovation project is part of the rational use of renewable energy through biomass. The innovation of this project is the coupling of an inline sugar detector to quantify the fermentable sugars obtained after hydrolysis in high quality final subcritical water. The raw materials will be subjected to hydrolysis with water under subcritical conditions to obtain sufficient hydrolyzate for the tests to continue production of 2G ethanol and or anaerobic digestion and biogas production. Glucose and ethanol, furfural and HMF concentrations will be quantified using HPLC equipment. (AU)

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Scientific publications (38)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
SGANZERLA, WILLIAM G.; AMPESE, LARISSA C.; PARISOTO, THUANNY A. C.; FORSTER-CARNEIRO, TANIA. Process intensification for the recovery of methane-rich biogas from dry anaerobic digestion of acai seeds. BIOMASS CONVERSION AND BIOREFINERY, . (18/05999-0, 18/14938-4, 19/26925-7)
DE OLIVEIRA, TATIANE C. G.; SGANZERLA, WILLIAM GUSTAVO; AMPESE, LARISSA CASTRO; SFORCA, BEATRIZ P.; GOLDBECK, ROSANA; FORSTER-CARNEIRO, TANIA. Sustainable valorization of apple waste in a biorefinery: a bibliometric analysis. BIOFUELS BIOPRODUCTS & BIOREFINING-BIOFPR, v. 16, n. 3, p. 29-pg., . (18/14938-4, 19/26925-7, 18/05999-0)
TENA, MIRIAM; BULLER, LUZ S.; SGANZERLA, WILLIAM G.; BERNI, MAURO; FORSTER-CARNEIRO, TANIA; SOLERA, ROSARIO; PEREZ, MONTSERRAT. Techno-economic evaluation of bioenergy production from anaerobic digestion of by-products from ethanol flex plants. FUEL, v. 309, . (20/10323-5, 19/26925-7, 18/05999-0, 18/14938-4)
BULLER, L. S.; SGANZERLA, W. G.; BERNI, M. D.; BRIGNOLI, S. C.; FORSTER-CARNEIRO, T.. esign and techno-economic analysis of a hybrid system for energy supply in a wastewater treatment plant: A decentralized energy strateg. Journal of Environmental Management, v. 305, . (18/05999-0, 20/10323-5, 19/26925-7, 15/50612-8, 18/14938-4)
SGANZERLA, WILLIAM G.; AMPESE, LARISSA C.; MUSSATTO, SOLANGE I.; FORSTER-CARNEIRO, TANIA. A bibliometric analysis on potential uses of brewer's spent grains in a biorefinery for the circular economy transition of the beer industry. BIOFUELS BIOPRODUCTS & BIOREFINING-BIOFPR, v. 15, n. 6, . (19/26925-7, 18/14938-4, 18/05999-0)
SGANZERLA, WILLIAM GUSTAVO; DA ROSA, CLEONICE GONCALVES; GOMES DA SILVA, ALINE PRISCILLA; FERRAREZE, JOCLEITA PERUZZO; AZEVEDO, MONIA STREMEL; FORSTER-CARNEIRO, TANIA; NUNES, MICHAEL RAMOS; DE LIMA VEECK, ANA PAULA. Application in situ of biodegradable films produced with starch, citric pectin and functionalized with feijoa (Acca sellowiana (Berg) Burret) extracts: An effective proposal for food conservation. International Journal of Biological Macromolecules, v. 189, p. 544-553, . (19/26925-7, 18/14938-4)
SGANZERLA, WILLIAM GUSTAVO; CASTRO, LUIZ EDUARDO NOCHI; DA ROSA, CLEONICE GONCALVES; ALMEIDA, ALINE DA ROSA; MACIEL-SILVA, FRANCISCO WESHLEY; KEMPE, PAULA REGINA GELINSKI; DE OLIVEIRA, ALEXANDRE LEITE RODRIGUES; FORSTER-CARNEIRO, TANIA; BERTOLDI, FABIANO CLEBER; BARRETO, PEDRO LUIZ MANIQUE; et al. Production of nanocomposite films functionalized with silver nanoparticles bioreduced with rosemary (Rosmarinus officinalis L.) essential oil. JOURNAL OF AGRICULTURE AND FOOD RESEARCH, v. 11, p. 10-pg., . (19/26925-7)
SGANZERLA, WILLIAM GUSTAVO; AMPESE, LARISSA CASTRO; MUSSATTO, SOLANGE I.; FORSTER-CARNEIRO, TANIA. Subcritical water pretreatment enhanced methane-rich biogas production from the anaerobic digestion of brewer's spent grains. ENVIRONMENTAL TECHNOLOGY, v. N/A, p. 19-pg., . (19/26925-7, 18/14938-4, 21/12762-9)
MACIEL-SILVA, FRANCISCO W.; VIGANO, JULIANE; CASTRO, LUIZ E. N.; SGANZERLA, WILLIAM GUSTAVO; BULLER, LUZ SELENE; MARTINEZ, JULIAN; ROSTAGNO, MAURICIO A.; FORSTER-CARNEIRO, TANIA. Pressurized liquid extraction coupled in-line with SPE and on-line with HPLC (PLE-SPExHPLC) for the recovery and purification of anthocyanins from SC-CO2 semi-defatted Acai (Euterpe oleracea). Food Research International, v. 160, p. 11-pg., . (20/10323-5, 20/15774-5, 18/14938-4, 18/05999-0, 19/26925-7, 18/14582-5)
SILLERO, LEONOR; GUSTAVO SGANZERLA, WILLIAM; FORSTER-CARNEIRO, TANIA; SOLERA, ROSARIO; PEREZ, MONTSERRAT. A bibliometric analysis of the hydrogen production from dark fermentation. INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, v. 47, n. 64, p. 24-pg., . (19/26925-7, 18/14938-4, 21/12762-9)
SGANZERLA, WILLIAM GUSTAVO; VIGANO, JULIANE; CASTRO, LUIZ EDUARDO NOCHI; MACIEL-SILVA, FRANCISCO WESHLEY; ROSTAGNO, MAURICIO A.; MUSSATTO, SOLANGE I.; FORSTER-CARNEIRO, TANIA. Recovery of sugars and amino acids from brewers' spent grains using subcritical water hydrolysis in a single and two sequential semi-continuous flow-through reactors. Food Research International, v. 157, p. 11-pg., . (19/26925-7, 20/15774-5, 18/05999-0, 19/13496-0)
ZARZZEKA, CAROLINE; GOLDONI, JONAS; MARAFON, FILOMENA; SGANZERLA, WILLIAM GUSTAVO; FORSTER-CARNEIRO, TANIA; BAGATINI, MARGARETE DULCE; COLPINI, LEDA MARIA SARAGIOTTO. Use of titanium dioxide nanoparticles for cancertreatment: A comprehensive review and bibliometric analysis. BIOCATALYSIS AND AGRICULTURAL BIOTECHNOLOGY, v. 50, p. 24-pg., . (19/26925-7, 18/14938-4)
SGANZERLA, WILLIAM GUSTAVO; DA SILVA, MARCOS FELLIPE; ZABOT, GIOVANI L.; GOLDBECK, ROSANA; MUSSATTO, SOLANGE I.; FORSTER-CARNEIRO, TANIA. Techno-economic assessment of subcritical water hydrolysis of brewer?s spent grains to recover xylo-oligosaccharides. JOURNAL OF SUPERCRITICAL FLUIDS, v. 196, p. 12-pg., . (19/26925-7, 19/08542-3, 18/14938-4, 21/12762-9)
SGANZERLA, WILLIAM GUSTAVO; TENA, MIRIAM; SILLERO, LEONOR; MAGRINI, FLAVIANE EVA; SOPHIATTI, IGOR VINICIUS MACHADO; GAIO, JULIANO; PAESI, SUELEN; FORSTER-CARNEIRO, TANIA; SOLERA, ROSARIO; PEREZ, MONTSERRAT. Application of Anaerobic Co-digestion of Brewery by-Products for Biomethane and Bioenergy Production in a Biorefinery Concept. BioEnergy Research, v. N/A, p. 14-pg., . (19/26925-7, 18/14938-4)
DA ROSA, RAFAEL GABRIEL; SGANZERLA, WILLIAM GUSTAVO; BARROSO, TIAGO LINHARES CRUZ TABOSA; CASTRO, LUIZ EDUARDO NOCHI; BERNI, MAURO DONIZETTI; FORSTER-CARNEIRO, TANIA. Sustainable bioprocess combining subcritical water pretreatment followed by anaerobic digestion for the valorization of jabuticaba (Myrciaria cauliflora) agro-industrial by-product in bioenergy and biofertilizer. FUEL, v. 334, p. 15-pg., . (19/26925-7, 20/16248-5, 21/04096-9)
BARROSO, TIAGO; SGANZERLA, WILLIAM; ROSA, RAFAEL; CASTRO, LUIZ; MACIEL-SILVA, FRANCISCO; ROSTAGNO, MAURICIO; FORSTER-CARNEIRO, TANIA. Semi-continuous flow-through hydrothermal pretreatment for the recovery of bioproducts from jabuticaba (Myrciaria cauliflora) agro-industrial by-product. Food Research International, v. 158, p. 12-pg., . (20/16248-5, 18/14582-5, 21/04096-9, 19/26925-7)
AMPESE, LARISSA CASTRO; ZIERO, HENRIQUE DI DOMENICO; VELASQUEZ, JEAN; SGANZERLA, WILLIAM GUSTAVO; MARTINS, GILBERTO; FORSTER-CARNEIRO, TANIA. Apple pomace management by anaerobic digestion and composting: a life cycle assessment. BIOFUELS BIOPRODUCTS & BIOREFINING-BIOFPR, v. 17, n. 1, p. 17-pg., . (21/08696-0, 18/14938-4, 19/26925-7, 21/12762-9)
SGANZERLA, WILLIAM GUSTAVO; TENA-VILLARES, MIRIAM; BULLER, LUZ SELENE; MUSSATTO, SOLANGE, I; FORSTER-CARNEIRO, TANIA. Dry Anaerobic Digestion of Food Industry by-Products and Bioenergy Recovery: A Perspective to Promote the Circular Economy Transition. WASTE AND BIOMASS VALORIZATION, v. 13, n. 5, p. 15-pg., . (18/05999-0, 19/26925-7, 18/14938-4, 20/10323-5)
BARROSO, TIAGO LINHARES CRUZ TABOSA; SGANZERLA, WILLIAM GUSTAVO; CASTRO, LUIZ EDUARDO NOCHI; FREIRIA, NICOLAS LUIS MOREIRA; BARBERO, GERARDO FERNANDEZ; LOVILLO, MIGUEL PALMA; ROSTAGNO, MAURICIO ARIEL; FORSTER-CARNEIRO, TANIA. Removal of 5-hydroxymethylfurfural from brewer's spent grains hydrolysates obtained by subcritical water hydrolysis: An approach using liquid-liquid extraction. JOURNAL OF SUPERCRITICAL FLUIDS, v. 201, p. 9-pg., . (21/04096-9, 18/14582-5, 18/14938-4, 20/16248-5, 19/26925-7)
LOPES AGUIAR, JAIME PAIVA; DA SILVA, EDSON PABLO; GOMES DA SILVA, ALINE PRISCILLA; SGANZERLA, WILLIAM GUSTAVO; XIAO, JIANBO; SOUZA, FRANCISCA DAS C. DO A.. Influence of freeze-drying treatment on the chemical composition of peppers (Capsicum L.) from the Brazilian Amazonia region. BIOCATALYSIS AND AGRICULTURAL BIOTECHNOLOGY, v. 38, . (19/26925-7)
SGANZERLA, WILLIAM GUSTAVO; BULLER, LUZ SELENE; MUSSATTO, I, SOLANGE; FORSTER-CARNEIRO, TANIA. Techno-economic assessment of bioenergy and fertilizer production by anaerobic digestion of brewer's spent grains in a biorefinery concept. JOURNAL OF CLEANER PRODUCTION, v. 297, . (18/05999-0, 19/26925-7, 18/14938-4, 20/10323-5)
SGANZERLA, WILLIAM GUSTAVO; DA SILVA, ALINE PRISCILLA GOMES. Uvaia (Eugenia pyriformis Cambess - Myrtaceae): An overview from the origin to recent developments in the food industry - A bibliometric analysis. JOURNAL OF AGRICULTURE AND FOOD RESEARCH, v. 10, p. 10-pg., . (19/26925-7)
NOCHI CASTRO, LUIZ EDUARDO; SGANZERLA, WILLIAM GUSTAVO; CRUZ TABOSA BARROSOA, TIAGO LINHARES; MACIEL-SILVA, FRANCISCO WESHLEY; SARAGIOTTO COLPINI, LEDA MARIA; STIVAL BITTENCOURT, PAULO RODRIGO; ROSTAGNO, MAURICIO A.; FORSTER-CARNEIRO, TANIA. Improving the semi-continuous flow-through subcritical water hydrolysis of grape pomace (Vitis vinifera L.) by pH and temperature control. JOURNAL OF SUPERCRITICAL FLUIDS, v. 196, p. 14-pg., . (21/04096-9, 18/14582-5, 18/14938-4, 19/26925-7, 20/16248-5)
MARTINS, MANOELA; SGANZERLA, WILLIAM GUSTAVO; FORSTER-CARNEIRO, TANIA; GOLDBECK, ROSANA. Recent advances in xylo-oligosaccharides production and applications: A comprehensive review and bibliometric analysis. BIOCATALYSIS AND AGRICULTURAL BIOTECHNOLOGY, v. 47, p. 16-pg., . (19/26925-7, 19/08542-3, 18/14938-4, 20/02871-2)
MARINHO, LEONARDO DE FREITAS; SGANZERLA, WILLIAM GUSTAVO; FERREIRA, VANESSA COSME; MORENO, JUVER ANDREY JIMENEZ; ROSTAGNO, MAURICIO ARIEL; FORSTER-CARNEIRO, TANIA. Advances in green extraction methods, biological properties, and applications of betanin and vitexin: An updated review and bibliometric analysis. BIOCATALYSIS AND AGRICULTURAL BIOTECHNOLOGY, v. 51, p. 17-pg., . (19/26925-7, 22/11690-7, 22/02305-2, 18/14938-4)
SGANZERLA, WILLIAM G.; AMPESE, LARISSA C.; PARISOTO, THUANNY A. C.; FORSTER-CARNEIRO, TANIA. Process intensification for the recovery of methane-rich biogas from dry anaerobic digestion of acai seeds. BIOMASS CONVERSION AND BIOREFINERY, v. N/A, p. 14-pg., . (18/05999-0, 19/26925-7, 18/14938-4)
DE SILVA, ALINE PRISCILLA GOMES; SGANZERLA, WILLIAM GUSTAVO; JACOMINO, ANGELO PEDRO; DA SILVA, EDSON PABLO; XIAO, JIANBO; SIMAL-GANDARA, JESUS. Chemical composition, bioactive compounds, and perspectives for the industrial formulation of health products from uvaia (Eugenia pyriformis Cambess - Myrtaceae): A comprehensive review. Journal of Food Composition and Analysis, v. 109, p. 10-pg., . (14/13473-7, 19/26925-7, 14/12606-3)
BULLER, LUZ SELENE; SGANZERLA, WILLIAM GUSTAVO; LIMA, MICHELE NUNES; MUENCHOW, KERRY E.; TIMKO, MICHAEL T.; FORSTER-CARNEIRO, TANIA. Ultrasonic pretreatment of brewers' spent grains for anaerobic digestion: Biogas production for a sustainable industrial development. JOURNAL OF CLEANER PRODUCTION, v. 355, p. 11-pg., . (18/05999-0, 19/26925-7, 20/10323-5, 18/14938-4)
GUSTAVO SGANZERLA, WILLIAM; SILLERO, LEONOR; FORSTER-CARNEIRO, TANIA; SOLERA, ROSARIO; PEREZ, MONTSERRAT. Determination of Anaerobic Co-fermentation of Brewery Wastewater and Brewer's Spent Grains for Bio-hydrogen Production. BioEnergy Research, v. N/A, p. 11-pg., . (18/14938-4, 19/26925-7, 21/12762-9)
SGANZERLA, WILLIAM GUSTAVO; ZABOT, GIOVANI LEONE; TORRES-MAYANGA, PAULO CESAR; BULLER, LUZ SELENE; MUSSATTO, I, SOLANGE; FORSTER-CARNEIRO, TANIA. Techno-economic assessment of subcritical water hydrolysis process for sugars production from brewer's spent grains. INDUSTRIAL CROPS AND PRODUCTS, v. 171, . (18/05999-0, 20/10323-5, 18/14938-4, 19/26925-7)
FERREIRA, SAMUEL F.; BULLER, LUZ S.; MACIEL-SILVA, FRANCISCO W.; SGANZERLA, WILLIAM G.; BERNI, MAURO D.; FORSTER-CARNEIRO, TANIA. Waste management and bioenergy recovery from acai processing in the Brazilian Amazonian region: a perspective for a circular economy. BIOFUELS BIOPRODUCTS & BIOREFINING-BIOFPR, v. 15, n. 1, p. 37-46, . (18/05999-0, 18/14938-4, 19/26925-7)
SGANZERLA, WILLIAM GUSTAVO; COSTA, JOSIEL MARTINS; TENA-VILLARES, MIRIAM; BULLER, LUZ SELENE; MUSSATTO, SOLANGE I.; FORSTER-CARNEIRO, TANIA. Dry Anaerobic Digestion of Brewer's Spent Grains toward a More Sustainable Brewery: Operational Performance, Kinetic Analysis, and Bioenergy Potential. FERMENTATION-BASEL, v. 9, n. 1, p. 15-pg., . (19/26925-7, 21/03950-6, 18/14938-4, 20/10323-5)
SILLERO, LEONOR; SGANZERLA, WILLIAM GUSTAVO; CARNEIRO, TANIA FORSTER; SOLERA, ROSARIO; PEREZ, MONTSERRAT. Techno-economic analysis of single-stage and temperature-phase anaerobic co-digestion of sewage sludge, wine vinasse, and poultry manure. Journal of Environmental Management, v. 325, p. 10-pg., . (19/26925-7, 18/14938-4)
BARROSO, TIAGO LINHARES CRUZ TABOSA; DA ROSA, RAFAEL GABRIEL; SGANZERLA, WILLIAM GUSTAVO; CASTRO, LUIZ EDUARDO NOCHI; MACIEL-SILVA, FRANCISCO WESHLEY; ROSTAGNO, MAURICIO ARIEL; FORSTER-CARNEIRO, TANIA. Hydrothermal pretreatment based on semi-continuous flow-through sequential reactors for the recovery of bioproducts from jabuticaba (Myrciaria cauliflora) peel. JOURNAL OF SUPERCRITICAL FLUIDS, v. 191, p. 14-pg., . (18/14582-5, 19/26925-7, 20/16248-5, 21/04096-9)
SGANZERLA, WILLIAM GUSTAVO; LACHOS-PEREZ, DANIEL; BULLER, LUZ SELENE; ZABOT, GIOVANI L.; FORSTER-CARNEIRO, TANIA. ost analysis of subcritical water pretreatment of sugarcane straw and bagasse for second-generation bioethanol production: a case study in a sugarcane mil. BIOFUELS BIOPRODUCTS & BIOREFINING-BIOFPR, v. 16, n. 2, . (18/14938-4, 20/10323-5, 19/26925-7, 18/05999-0)
ZIERO, HENRIQUE DI DOMENICO; AMPESE, LARISSA CASTRO; SGANZERLA, WILLIAM G.; TORRES-MAYANGA, PAULO C.; TIMKO, MICHAEL T.; MUSSATTO, I, SOLANGE; FORSTER-CARNEIRO, T.. Subcritical water hydrolysis of poultry feathers for amino acids production. JOURNAL OF SUPERCRITICAL FLUIDS, v. 181, . (18/14938-4, 19/26925-7, 18/05999-0)
AMPESE, LARISSA CASTRO; SGANZERLA, WILLIAM GUSTAVO; ZIERO, HENRIQUE DI DOMENICO; COSTA, JOSIEL MARTINS; MARTINS, GILBERTO; FORSTER-CARNEIRO, TANIA. Valorization of apple pomace for biogas production: a leading anaerobic biorefinery approach for a circular bioeconomy. BIOMASS CONVERSION AND BIOREFINERY, v. N/A, p. 15-pg., . (18/14938-4, 19/26925-7, 21/03950-6)
AMPESE, LARISSA CASTRO; DE GOUVEA, MIRIAM TVRZSKA; BULLER, LUZ SELENE; SGANZERLA, WILLIAM GUSTAVO; ROSA, MARIA THEREZA DE MORAES GOMES; FORSTER-CARNEIRO, TANIA. Using thermodynamic models for bioenergy recovery and generation assessment: a case study with acai and macauba by-products. BIOMASS CONVERSION AND BIOREFINERY, v. N/A, p. 16-pg., . (20/10323-5, 18/14938-4, 19/26925-7)
Academic Publications
(References retrieved automatically from State of São Paulo Research Institutions)
SGANZERLA, William Gustavo. Hidrólise em água subcrítica de bagaço de malte: um pré-tratamento sustentável para produção de produtos de valor agregado e bioenergia em um conceito de biorrefinaria. 2023. Doctoral Thesis - Universidade Estadual de Campinas (UNICAMP). Faculdade de Engenharia de Alimentos Campinas, SP.

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