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Alternative analytical techniques and in vitro digestion assays to special foods

Grant number: 22/03268-3
Support Opportunities:Regular Research Grants
Start date: December 01, 2022
End date: November 30, 2024
Field of knowledge:Agronomical Sciences - Food Science and Technology - Food Science
Principal Investigator:Juliana Azevedo Lima Pallone
Grantee:Juliana Azevedo Lima Pallone
Host Institution: Faculdade de Engenharia de Alimentos (FEA). Universidade Estadual de Campinas (UNICAMP). Campinas , SP, Brazil
Associated researchers:Ana Paula Rebellato ; Bruno Lemos Batista ; Débora Parra Baptista Freitas ; Mirna Lúcia Gigante ; Patrícia Valderrama ; Ralf Greiner

Abstract

The research project aims to presents the application of alternative analytical techniques, considered emerging, such as near infrared spectroscopy, UV-visible spectrophotometry associated with chemometric tools for the evaluation of the potential for discrimination of special, green and roasted canephore coffees, produced in different regions of Brazil and fraud detection; and perform in vitro digestion assays to assess the bioaccessibility of essential elements in plant based foods and organic and A2 milk and correlate with some components of the products, both as an unpublished proposals. It is a continuation of the projects carried out by the research group, with the use of new matrices and different applications of spectroanalytic techniques and the simulation of in vitro digestion. Recently, 30 scientific manuscripts, in addition to a patent deposit, an award at an international congress, were obtained as results of this line of research. Fine/special coffee, plant based and organic foods were named as "special" in the project title, as they differ from traditional "similars". The techniques considered alternative, are associated with green analytical chemistry, allow direct analysis, with quick answers, after performing exploratory analysis and building classification or multivariate calibration models. However, studies with special canephore coffees as a new application are unprecedented and will contribute to the growth of the market for this product, including indigenous coffees produced in Rondônia. In another context, data on the availability of essential elements, whose deficiencies are considered serious worldwide public health problems, in special foods indicated the basis for nutritional assessments and contribute with relevant considerations regarding possible or expected benefits or healthiness associated with the consumption of these differentiated products. (AU)

Articles published in Agência FAPESP Newsletter about the research grant:
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Scientific publications (15)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
BAQUETA, MICHEL ROCHA; VALDERRAMA, PATRICIA; MANDRONE, MANUELA; POLI, FERRUCCIO; COQUEIRO, ALINE; COSTA-SANTOS, AUGUSTO CESAR; REBELLATO, ANA PAULA; LUZ, GISELE MARCONDES; ROCHA, RODRIGO BARROS; PALLONE, JULIANA AZEVEDO LIMA; et al. 1H NMR, FAAS, portable NIR, benchtop NIR, and ATR-FTIR-MIR spectroscopies for characterizing and discriminating new Brazilian Canephora coffees in a multi-block analysis perspective. CHEMOMETRICS AND INTELLIGENT LABORATORY SYSTEMS, v. 240, p. 11-pg., . (19/21062-0, 22/03268-3, 22/04068-8)
BAQUETA, MICHEL ROCHA; MARINI, FEDERICO; ROCHA, RODRIGO BARROS; VALDERRAMA, PATRICIA; PALLONE, JULIANA AZEVEDO LIMA. Authentication and discrimination of new Brazilian Canephora coffees with geographical indication using a miniaturized near-infrared spectrometer. Food Research International, v. 172, p. 10-pg., . (19/21062-0, 22/03268-3, 22/04068-8)
COSTA-SANTOS, AUGUSTO CESAR; REBELLATO, ANA PAULA; LUZ, GISELE MARCONDES; PALLONE, JULIANA AZEVEDO LIMA. A2 milk: Bioaccessibility of essential minerals and the release of amino groups under static in vitro digestion conditions. Food Research International, v. 186, p. 10-pg., . (22/03268-3)
BAQUETA, MICHEL ROCHA; MARINI, FEDERICO; TEIXEIRA, ALEXSANDRO LARA; GOULART, BRUNO HENRIQUE FERMINO; PILAU, EDUARDO JORGE; VALDERRAMA, PATRICIA; PALLONE, JULIANA AZEVEDO LIMA. Spectroscopic and sensory characterization of Brazilian Coffea canephora terroir and botanical varieties produced in the Amazon and Espirito Santo implementing multi-block approaches. Journal of Food Composition and Analysis, v. 133, p. 12-pg., . (22/04068-8, 22/03268-3, 19/21062-0)
BAQUETA, MICHEL ROCHA; POSTIGO, MATHEUS PEREIRA; ALVES, ENRIQUE ANASTACIO; DE MORAES NETO, VENANCIO FERREIRA; VALDERRAMA, PATRICIA; PALLONE, JULIANA AZEVEDO LIMA; DINIZ, PAULO HENRIQUE GONCALVES DIAS. Authentication of indigenous Brazilian specialty canephora coffees using smartphone image analysis. Food Research International, v. 196, p. 8-pg., . (22/04068-8, 22/03268-3, 19/21062-0)
DE MORAES-NETO, VENANCIO FERREIRA; COSTA-SANTOS, AUGUSTO CESAR; PALLONE, JULIANA AZEVEDO LIMA. Portable Near-Infrared Spectrometer in Tandem with Chemometrics as an Option for the Authenticating Commercial A2 Bovine Milk. FOOD ANALYTICAL METHODS, v. N/A, p. 10-pg., . (22/03268-3)
COSTA-SANTOS, AUGUSTO CESAR; REBELLATO, ANA PAULA; ORLANDO, EDUARDO ADILSON; PALLONE, JULIANA AZEVEDO LIMA. Characterization and estimation of the bioaccessibility of essential elements in organic milk by INFOGEST protocol. Food Chemistry, v. 433, p. 9-pg., . (22/03268-3)
BAQUETA, MICHEL ROCHA; VALDERRAMA, PATRICIA; ALVES, ENRIQUE ANASTACIO; PALLONE, JULIANA AZEVEDO LIMA; MARINI, FEDERICO. Discrimination of Robusta Amazonico coffee farmed by indigenous and non-indigenous people in Amazon: comparing benchtop and portable NIR using ComDim and duplex. ANALYST, v. 148, n. 7, p. 10-pg., . (19/21062-0, 22/03268-3, 22/04068-8)
BAQUETA, MICHEL ROCHA; ALVES, ENRIQUE ANASTACIO; VALDERRAMA, PATRICIA; PALLONE, JULIANA AZEVEDO LIMA. Brazilian Canephora coffee evaluation using NIR spectroscopy and discriminant chemometric techniques. Journal of Food Composition and Analysis, v. 116, p. 10-pg., . (19/21062-0, 22/03268-3)
DE MORAES-NETO, VENANCIO FERREIRA; BAQUETA, MICHEL ROCHA; CARAMES, ELEM TAMIRYS DOS SANTOS; DE SANTANA, FELIPE BACHION; ALVES, ENRIQUE ANASTACIO; PALLONE, JULIANA AZEVEDO LIMA. Discrimination of Brazilian green canephora coffee beans by ultraviolet-visible - visible spectroscopy as a non-target analysis: A tool for recognizing geographical indications. Microchemical Journal, v. 202, p. 7-pg., . (22/03268-3)
BAQUETA, MICHEL ROCHA; PALLONE, JULIANA AZEVEDO LIMA; PILAU, EDUARDO JORGE; GOULARTC, BRUNO HENRIQUE FERMINO; ROCHA, RODRIGO BARROS; VALDERRAMA, PATRICIA; RUTLEDGE, DOUGLAS N.. Enhancing mass spectrometry interpretability by ComDim-ICA multi-block analysis: Geographical and varietal traceability of Brazilian Coffea canephora. Talanta, v. 281, p. 9-pg., . (22/04068-8, 22/03268-3, 19/21062-0)
LUZ, GISELE MARCONDES; COSTA-SANTOS, AUGUSTO CESAR; MORAES-NETO, VENANCIO FERREIRA; PALLONE, JULIANA AZEVEDO LIMA. Nutritional quality of plant-based meat and dairy alternatives, and new front-of-package labeling (FOPL) in Brazil. JOURNAL OF FOOD SCIENCE AND TECHNOLOGY-MYSORE, v. 61, n. 5, p. 11-pg., . (22/03268-3)
BAQUETA, MICHEL ROCHA; COSTA-SANTOS, AUGUSTO CESAR; REBELLATO, ANA PAULA; LUZ, GISELE MARCONDES; LIMA PALLONE, JULIANA AZEVEDO; MARINI, FEDERICO; TEIXEIRA, ALEXSANDRO LARA; RUTLEDGE, DOUGLAS N.; VALDERRAMA, PATRICIA. Independent components-discriminant analysis for discrimination of Brazilian Canephora coffees based on their inorganic fraction: A preliminary chemometric study. Microchemical Journal, v. 196, p. 8-pg., . (22/04068-8, 22/03268-3, 19/21062-0)
BAQUETA, MICHEL ROCHA; RUTLEDGE, DOUGLAS N.; ALVES, ENRIQUE ANASTACIO; MANDRONE, MANUELA; POLI, FERRUCCIO; COQUEIRO, ALINE; COSTA-SANTOS, AUGUSTO CESAR; REBELLATO, ANA PAULA; LUZ, GISELE MARCONDES; GOULART, BRUNO HENRIQUE FERMINO; et al. Multiplatform Path-ComDim study of Capixaba, indigenous and non-indigenous Amazonian Canephora coffees. Food Chemistry, v. 463, p. 11-pg., . (22/04068-8, 22/03268-3, 19/21062-0)
BAQUETA, MICHEL ROCHA; DINIZ, PAULO HENRIQUE GONSALVES DIAS; PEREIRA, LUCAS LOUZADA; ALMEIDA, FRANCISCO LUCAS CHAVES; VALDERRAMA, PATRICIA; PALLONE, JULIANA AZEVEDO LIMA. An overview on the Brazilian Coffea canephora scenario and the current chemometrics-based spectroscopic research. Food Research International, v. 194, p. 22-pg., . (22/04068-8, 22/03268-3, 19/21062-0)