Purification of jabuticaba waste extracts by adsorbents and biochar using supercritical technology

• Grant number: 20/16248-5
• Support Opportunities: Scholarships in Brazil - Master
• Start date: March 01, 2021
• End date: July 31, 2023
• Field of knowledge: Agronomical Sciences - Food Science and Technology - Food Engineering
• Principal Investigator: Tânia Forster Carneiro
• Grantee: Tiago Linhares Cruz Tabosa Barroso
• Host Institution: Faculdade de Engenharia de Alimentos (FEA). Universidade Estadual de Campinas (UNICAMP). Campinas , SP, Brazil
• Associated research grant: 18/14938-4 - Waste2energy: integration of supercritical technologies and anaerobic digestion through an automated system for the production of biofuel precursors, AP.JP2
• Associated scholarship(s): 22/02039-0 - Recovery biocomponents of jabuticaba peel through microwave-assisted solid phase extraction (MASPE) and developing a rapid method of analysis in ultra-high performance liquid chromatography, BE.EP.MS

Abstract

This research and technological innovation project is part of the rational use of renewable energy through biomass. Currently, technical solutions for the benefit of biomass and waste, enabling fuel production, energy, and chemical insums are already regularized. The innovation of this project lies in the coupling of an inline detector of adsorbents and biochar obtained after extraction in a high quality final subcritical water for purification of components and online ana lise of the results through the coupling of HPLC in the pilot plant. This work aims to integrate the extraction and purification processes in a sub/supercritical technology unit. After pretreatment, the raw material is subjected to extraction with water to subcritical conditions to obtain an extract; the continuation passes through a column containing several types of biochar and adsorbents for purification. It will be possible to get as curved results of the kinetics of retention of compounds in the solution, identify the behavior of the adsorbent concerning saturation or obstruction, and the presence of some preferential paths in the column bed filled with the adsorbent and or biochar. (AU)

Scientific publications

(7)

(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)

BARROSO, TIAGO L. C. T.; CASTRO, LUIZ E. N.; F. BARBERO, GERARDO; PALMA, MIGUEL; CARRERA, CEFERINO; ROSTAGNO, MAURICIO A.; FORSTER-CARNEIRO, TANIA. Optimization of a Microwave-Assisted Extraction Method for the Recovery of the Anthocyanins from Jabuticaba By-Products. AGRONOMY-BASEL, v. 13, n. 2, p. 13-pg., 2023-02-01. (22/02039-0, 18/14938-4, 20/16248-5, 18/14582-5, 21/04096-9)

BARROSO, TIAGO LINHARES CRUZ TABOSA; DA ROSA, RAFAEL GABRIEL; SGANZERLA, WILLIAM GUSTAVO; CASTRO, LUIZ EDUARDO NOCHI; MACIEL-SILVA, FRANCISCO WESHLEY; ROSTAGNO, MAURICIO ARIEL; FORSTER-CARNEIRO, TANIA. Hydrothermal pretreatment based on semi-continuous flow-through sequential reactors for the recovery of bioproducts from jabuticaba (Myrciaria cauliflora) peel. JOURNAL OF SUPERCRITICAL FLUIDS, v. 191, p. 14-pg., 2022-10-19. (18/14582-5, 19/26925-7, 20/16248-5, 21/04096-9)

FERREIRA, VANESSA COSME; SGANZERLA, WILLIAM GUSTAVO; BARROSO, TIAGO LINHARES CRUZ TABOSA; CASTRO, LUIZ EDUARDO NOCHI; COLPINI, LEDA MARIA SARAGIOTTO; FORSTER-CARNEIRO, TANIA. Sustainable valorization of pitaya (Hylocereus spp.) peel in a semi-continuous high-pressure hydrothermal process to recover value-added products. Food Research International, v. 173, p. 12-pg., 2023-11-01. (22/02305-2, 21/04096-9, 18/14582-5, 20/16248-5)

DA ROSA, RAFAEL GABRIEL; SGANZERLA, WILLIAM GUSTAVO; BARROSO, TIAGO LINHARES CRUZ TABOSA; CASTRO, LUIZ EDUARDO NOCHI; BERNI, MAURO DONIZETTI; FORSTER-CARNEIRO, TANIA. Sustainable bioprocess combining subcritical water pretreatment followed by anaerobic digestion for the valorization of jabuticaba (Myrciaria cauliflora) agro-industrial by-product in bioenergy and biofertilizer. FUEL, v. 334, p. 15-pg., 2023-02-15. (19/26925-7, 20/16248-5, 21/04096-9)

BARROSO, TIAGO; SGANZERLA, WILLIAM; ROSA, RAFAEL; CASTRO, LUIZ; MACIEL-SILVA, FRANCISCO; ROSTAGNO, MAURICIO; FORSTER-CARNEIRO, TANIA. Semi-continuous flow-through hydrothermal pretreatment for the recovery of bioproducts from jabuticaba (Myrciaria cauliflora) agro-industrial by-product. Food Research International, v. 158, p. 12-pg., 2022-06-28. (20/16248-5, 18/14582-5, 21/04096-9, 19/26925-7)

BARROSO, TIAGO LINHARES CRUZ TABOSA; SGANZERLA, WILLIAM GUSTAVO; CASTRO, LUIZ EDUARDO NOCHI; FREIRIA, NICOLAS LUIS MOREIRA; BARBERO, GERARDO FERNANDEZ; LOVILLO, MIGUEL PALMA; ROSTAGNO, MAURICIO ARIEL; FORSTER-CARNEIRO, TANIA. Removal of 5-hydroxymethylfurfural from brewer's spent grains hydrolysates obtained by subcritical water hydrolysis: An approach using liquid-liquid extraction. JOURNAL OF SUPERCRITICAL FLUIDS, v. 201, p. 9-pg., 2023-06-13. (21/04096-9, 18/14582-5, 18/14938-4, 20/16248-5, 19/26925-7)

NOCHI CASTRO, LUIZ EDUARDO; SGANZERLA, WILLIAM GUSTAVO; CRUZ TABOSA BARROSOA, TIAGO LINHARES; MACIEL-SILVA, FRANCISCO WESHLEY; SARAGIOTTO COLPINI, LEDA MARIA; STIVAL BITTENCOURT, PAULO RODRIGO; ROSTAGNO, MAURICIO A.; FORSTER-CARNEIRO, TANIA. Improving the semi-continuous flow-through subcritical water hydrolysis of grape pomace (Vitis vinifera L.) by pH and temperature control. JOURNAL OF SUPERCRITICAL FLUIDS, v. 196, p. 14-pg., 2023-02-28. (21/04096-9, 18/14582-5, 18/14938-4, 19/26925-7, 20/16248-5)

Academic Publications

(References retrieved automatically from State of São Paulo Research Institutions)

BARROSO, Tiago Linhares Cruz Tabosa. Pré-tratamento hidrotérmico baseado em configurações em reator unitário e sequencial de fluxo semicontínuo para a recuperação de biocompostos da casca da jabuticaba (Myrciaria cauliflora). 2023. Master's Dissertation - Universidade Estadual de Campinas (UNICAMP). Faculdade de Engenharia de Alimentos Campinas, SP.