A techno-economic evaluation of emerging technologies and green solvents coupling to the two-dimensional system of extraction, separation and analysis to obtain phenolic compounds from waste of the coffee and plant-based beverages industry

• Grant number: 21/12264-9
• Support Opportunities: Scholarships in Brazil - Post-Doctoral
• Start date: June 01, 2022
• End date: May 31, 2026
• Field of knowledge: Agronomical Sciences - Food Science and Technology - Food Engineering
• Principal Investigator: Maurício Ariel Rostagno
• Grantee: Monique Martins Strieder
• Host Institution: Faculdade de Ciências Aplicadas (FCA). Universidade Estadual de Campinas (UNICAMP). Limeira , SP, Brazil
• Associated research grant: 18/14582-5 - Development of a two-dimensional extraction, separation and analysis system for evaluating the bioactivity of phytochemicals, AP.JP2
• Associated scholarship(s): 23/05722-6 - Biorefinery of the vegetable almond and peanut-based milk processes: study of technologies and alternative solvents to obtain bioactive compounds from their solid residues, BE.EP.PD

Abstract

Consumer demand for healthier products that generate less impact on natural resources has boosted the development of innovative ingredients and processes. Therefore, green technologies and solvents can be chosen to extract phenolic compounds from industrial waste, allowing the production of a high added value product and reducing waste disposal. The coupling of technologies and reusable solvents also can be a good strategy for developing more efficient processes. They can allow the extraction of compounds with greater purity in a lower time, using less energy, generating less impact on the environment. Thus, this project aims to study the coupling of high-intensity ultrasound and gas expanded liquids technologies, as well as the reusable Deep Natural Eutectics Solvents (NADES) and Ionic Liquids (ILs) to the bidimensional system of extraction, separation, and analysis proposed by the project in development Jovem Pesquisador - Fase 2 (18/14582-5). For this, will be used coffee and almond husks as sources of phenolic compounds. Different configurations of technologies, solvents, and operational parameters will also be studied to obtain the phenolic compounds. Moreover, is proposed carried out part of this project at the Universidad Autónoma de Madrid under the supervision of Professor Elena Ibáñez, who has experience in using NADES to obtain bioactive compounds. Thus, it is intended to demonstrate the techno-economic potential that the bidimensional system can achieve using industrial waste to produce purer compounds, coupled technologies that can reduce energy expenditure, and more efficient and reusable solvents. (AU)

Scientific publications

(12)

(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)

SILVA, KLYCIA FIDELIS CERQUEIRA E; STRIEDER, MONIQUE MARTINS; PINTO, MARIANA BARRETO CARVALHAL; ROSTAGNO, MAURICIO ARIEL; HUBINGER, MIRIAM DUPAS. Processing Strategies for Extraction and Concentration of Bitter Acids and Polyphenols from Brewing By-Products: A Comprehensive Review. PROCESSES, v. 11, n. 3, p. 29-pg., 2023-03-01. (21/12264-9, 21/06863-7, 19/27354-3)

COSTA, JOSIEL MARTINS; STRIEDER, MONIQUE MARTINS; SALDANA, MARLENY D. A.; ROSTAGNO, MAURICIO ARIEL; FORSTER-CARNEIRO, TANIA. Recent Advances in the Processing of Agri-food By-products by Subcritical Water. Food and Bioprocess Technology, v. N/A, p. 20-pg., 2023-04-01. (18/14582-5, 18/14938-4, 21/12264-9, 21/03950-6)

VIGANO, JULIANE; STRIEDER, MONIQUE MARTINS; PIZANI, RODRIGO S.; CONTIERI, LETICIA S.; MESQUITA, LEONARDO M. DE SOUZA; ROSTAGNO, MAURICIO A.. Application of an integrative system (2D PLExHPLC-PDA) for bioactive compound extraction and online quantification: Advantages, validation, and considerations. Analytica Chimica Acta, v. 1272, p. 9-pg., 2023-06-15. (18/14582-5, 20/08421-9, 20/15774-5, 19/13496-0, 21/12264-9, 20/03623-2, 20/04067-6)

MARTINS STRIEDER, MONIQUE; MENDIOLA, JOSE; COKDINLEYEN, MELIS; VALDES, ALBERTO; BRAGAGNOLO, FELIPE SANCHEZ; BALBINOT FILHO, CLOVIS A.; LANZA, MARCELO; SALVADOR FERREIRA, SANDRA REGINA; CIFUENTES, ALEJANDRO; ROSTAGNO, MAURICIO ARIEL; et al. Sustainable valorization of almond and peanut plant-based milk cakes: The use of terpenoid mixtures as ready-to-use solvents to enhance supercritical CO₂ extraction. Food Chemistry, v. 479, p. 10-pg., 2025-07-01. (21/12264-9, 18/14582-5, 22/10469-5, 23/12621-1, 19/13496-0, 23/05722-6)

MESQUITA, LEONARDO M. DE SOUZA; CONTIERI, LETICIA S.; A. E SILVA, FRANCISCA; BAGINI, RAFAEL HENRIQUE; BRAGAGNOLO, FELIPE S.; STRIEDER, MONIQUE M.; SOSA, FILIPE H. B.; SCHAEFFER, NICOLAS; FREIRE, MARA G.; VENTURA, SONIA P. M.; et al. Path2Green: introducing 12 green extraction principles and a novel metric for assessing sustainability in biomass valorization. GREEN CHEMISTRY, v. 26, n. 19, p. 21-pg., 2024-08-12. (20/15774-5, 21/11022-1, 15/00658-1, 20/08421-9, 13/04304-4, 23/12621-1, 22/10469-5, 20/03623-2, 19/13496-0, 21/11023-8, 21/12264-9, 18/14582-5, 23/05722-6)

PIZANI, RODRIGO S.; VIGANO, JULIANE; CONTIERI, LETICIA S.; STRIEDER, MONIQUE M.; KAMIKAWASHI, RENAN K.; VILEGAS, WAGNER; MESQUITA, LEONARDO M. DE SOUZA; ROSTAGNO, MAURICIO A.. New selective and sustainable ultrasound-assisted extraction procedure to recover carnosic and rosmarinic acids from Rosmarinus officinalis by sequential use of bio-based solvents. Food Chemistry, v. 435, p. 11-pg., 2023-09-30. (20/08421-9, 20/04067-6, 20/03623-2, 19/13496-0, 21/12264-9, 18/14582-5)

STRIEDER, MONIQUE MARTINS; BRAGAGNOLO, FELIPE SANCHEZ; PIZANI, RODRIGO S.; ROSTAGNO, MAURICIO ARIEL. The impact of using an expansion gas with high-intensity ultrasound on the pressurized liquid extraction of bioactive compounds from an industrial coffee solid residue. INNOVATIVE FOOD SCIENCE & EMERGING TECHNOLOGIES, v. 92, p. 12-pg., 2024-01-26. (20/04067-6, 22/10469-5, 19/13496-0, 21/12264-9, 18/14582-5)

STRIEDER, MONIQUE MARTINS; VARDANEGA, RENATA; MORAES, MOYSES NAVES; SILVA, ERIC KEVEN; MEIRELES, MARIA ANGELA A.. One-step ultrasound-assisted recovery of yellow-orange-red natural coloring from defatted annatto seeds: A cleaner processing alternative. ULTRASONICS SONOCHEMISTRY, v. 107, p. 10-pg., 2024-05-21. (23/01876-9, 15/13299-0, 23/05722-6, 21/12264-9)

STRIEDER, MONIQUE MARTINS; SANCHES, VITOR LACERDA; ROSTAGNO, MAURICIO ARIEL. Simultaneous extraction, separation, and analysis of 5-caffeoylquinic acid and caffeine from coffee co-product by PLE-SPE x HPLC-PDA two-dimensional system. Food Research International, v. 175, p. 14-pg., 2023-11-16. (19/13496-0, 18/14582-5, 21/12264-9)

DE OLIVEIRA, ISADORA LOPES; STRIEDER, MONIQUE MARTINS; BRAGAGNOLO, FELIPE SANCHEZ; SANCHES, VITOR LACERDA; MESQUITA, LEONARDO MENDES DE SOUZA; VIGANO, JULIANE; ROSTAGNO, MAURICIO ARIEL. Selective Separation of α-Punicalagin, β-Punicalagin, and Ellagic Acid from Pomegranate Husk Aqueous Extract by an Optimized Adsorption Process Employing a (Deep) Eutectic Solvent. Food and Bioprocess Technology, v. N/A, p. 12-pg., 2024-09-28. (21/11022-1, 20/08421-9, 22/10469-5, 21/12264-9, 19/13496-0, 21/13638-0, 18/14582-5, 23/05722-6)

MOREIRA, MARIELE RODRIGUES; SANCHES, VITOR LACERDA; STRIEDER, MONIQUE MARTINS; ROSTAGNO, MAURICIO ARIEL; CAPITANI, CAROLINE DARIO. Vegan brownie enriched with phenolic compounds obtained from a chia (Salvia hipanica L.) coproduct: Nutritional, technological, and functional characteristics and sensory acceptance. INTERNATIONAL JOURNAL OF GASTRONOMY AND FOOD SCIENCE, v. 34, p. 11-pg., 2023-11-09. (19/13496-0, 18/14582-5, 21/12264-9)

STRIEDER, MONIQUE MARTINS; PINAS, JEAN AGUSTIN VELASQUEZ; AMPESE, LARISSA CASTRO; COSTA, JOSIEL MARTINS; CARNEIRO, TANIA FORSTER; ROSTAGNO, MAURICIO ARIEL. Coffee biorefinery: The main trends associated with recovering valuable compounds from solid coffee residues. JOURNAL OF CLEANER PRODUCTION, v. 415, p. 16-pg., 2023-06-17. (21/08696-0, 21/03950-6, 18/14582-5, 19/13496-0, 18/14938-4, 21/12264-9)